3-(2,2-diethoxyethyl)-5-(2-dimethylaminoethen-1-yl)-1,7-diphenyl-2,6-dicarbethoxy-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

Base Information

• Chemical Name: 3-(2,2-diethoxyethyl)-5-(2-dimethylaminoethen-1-yl)-1,7-diphenyl-2,6-dicarbethoxy-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene
• CAS No.: 1418012-39-1
• Molecular Formula: C₃₇H₄₂BF₂N₃O₆
• Molecular Weight: 673.565
• Mol file: 1418012-39-1.mol

Synonyms:3-(2,2-diethoxyethyl)-5-(2-dimethylaminoethen-1-yl)-1,7-diphenyl-2,6-dicarbethoxy-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

Chemical Property of 3-(2,2-diethoxyethyl)-5-(2-dimethylaminoethen-1-yl)-1,7-diphenyl-2,6-dicarbethoxy-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-(2,2-diethoxyethyl)-5-(2-dimethylaminoethen-1-yl)-1,7-diphenyl-2,6-dicarbethoxy-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

There total 2 articles about 3-(2,2-diethoxyethyl)-5-(2-dimethylaminoethen-1-yl)-1,7-diphenyl-2,6-dicarbethoxy-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

3-(2,2-diethoxyethyl)-5-methyl-1,7-diphenyl-2,6-dicarbethoxy-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene (1418012-38-0) + N,N-dimethyl-formamide dimethyl acetal (4637-24-5) → 3-(2,2-diethoxyethyl)-5-(2-dimethylaminoethen-1-yl)-1,7-diphenyl-2,6-dicarbethoxy-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene (1418012-39-1)

Guidance literature:

With acetic anhydride; In o-xylene; for 0.0166667h; Reflux;

DOI:10.1039/c2ob27004h

Reference yield:

(5-methyl-1,7-diphenyl-2,6-dicarbethoxy-4,4-difluoro-4-bora-3a,4a-diaza-s-indacen-3-yl)acetaldehyde → 3-(2,2-diethoxyethyl)-5-(2-dimethylaminoethen-1-yl)-1,7-diphenyl-2,6-dicarbethoxy-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene (1418012-39-1)

Guidance literature:

Multi-step reaction with 2 steps

1: trifluoroacetic acid / 5 h / Reflux

2: acetic anhydride / o-xylene / 0.02 h / Reflux

With acetic anhydride; trifluoroacetic acid; In o-xylene;

DOI:10.1039/c2ob27004h

Reference yield: 83.0%

3-(2,2-diethoxyethyl)-5-(2-dimethylaminoethen-1-yl)-1,7-diphenyl-2,6-dicarbethoxy-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene (1418012-39-1) → 3,5-bis(2-formylmethyl)-1,7-diphenyl-2,6-dicarbethoxy-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene (1418012-36-8)

Guidance literature:

With hydrogenchloride; water; at 20 ℃; for 18h;

DOI:10.1039/c2ob27004h

upstream raw materials:

3-(2,2-diethoxyethyl)-5-methyl-1,7-diphenyl-2,6-dicarbethoxy-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

N,N-dimethyl-formamide dimethyl acetal

Downstream raw materials:

3,5-bis(2-formylmethyl)-1,7-diphenyl-2,6-dicarbethoxy-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

3,5-bis(2-acetoxyethen-1-yl)-1,7-diphenyl-2,6-dicarbethoxy-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

3-(2-acetoxyethen-1-yl)-5-(2-phenylaminoethen-1-yl)-1,7-diphenyl-2,6-dicarbethoxy-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

3,5-bis(2-chloroethen-1-yl)-1,7-diphenyl-2,6-dicarbethoxy-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene