3-(2-acetoxyethen-1-yl)-5-(2-phenylaminoethen-1-yl)-1,7-diphenyl-2,6-dicarbethoxy-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

Base Information

• Chemical Name: 3-(2-acetoxyethen-1-yl)-5-(2-phenylaminoethen-1-yl)-1,7-diphenyl-2,6-dicarbethoxy-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene
• CAS No.: 1418012-41-5
• Molecular Formula: C₃₉H₃₄BF₂N₃O₆
• Molecular Weight: 689.523
• Mol file: 1418012-41-5.mol

Synonyms:

Chemical Property of 3-(2-acetoxyethen-1-yl)-5-(2-phenylaminoethen-1-yl)-1,7-diphenyl-2,6-dicarbethoxy-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-(2-acetoxyethen-1-yl)-5-(2-phenylaminoethen-1-yl)-1,7-diphenyl-2,6-dicarbethoxy-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

There total 7 articles about 3-(2-acetoxyethen-1-yl)-5-(2-phenylaminoethen-1-yl)-1,7-diphenyl-2,6-dicarbethoxy-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

3,5-bis(2-acetoxyethen-1-yl)-1,7-diphenyl-2,6-dicarbethoxy-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene (1418012-40-4) + aniline (62-53-3) → 3-(2-acetoxyethen-1-yl)-5-(2-phenylaminoethen-1-yl)-1,7-diphenyl-2,6-dicarbethoxy-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene (1418012-41-5)

Guidance literature:

In acetonitrile; Heating;

DOI:10.1039/c2ob27004h

Reference yield:

C32H29BF2N2O6 (1206782-13-9) → 3-(2-acetoxyethen-1-yl)-5-(2-phenylaminoethen-1-yl)-1,7-diphenyl-2,6-dicarbethoxy-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene (1418012-41-5)

Guidance literature:

Multi-step reaction with 5 steps

1: acetic anhydride / o-xylene / 0.02 h / Reflux

2: water / acetonitrile / 1 h

3: water; trifluoroacetic acid / 0.02 h / Reflux

4: N,N-dimethyl-formamide / 0.02 h / Reflux

5: acetonitrile / Heating

With water; acetic anhydride; N,N-dimethyl-formamide; trifluoroacetic acid; In o-xylene; acetonitrile;

DOI:10.1039/c2ob27004h

Reference yield:

3-(2,2-diethoxyethyl)-5-(2-dimethylaminoethen-1-yl)-1,7-diphenyl-2,6-dicarbethoxy-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene (1418012-39-1) → 3-(2-acetoxyethen-1-yl)-5-(2-phenylaminoethen-1-yl)-1,7-diphenyl-2,6-dicarbethoxy-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene (1418012-41-5)

Guidance literature:

Multi-step reaction with 3 steps

1: hydrogenchloride; water / 18 h / 20 °C

2: N,N-dimethyl-formamide / 0.02 h / Reflux

3: acetonitrile / Heating

With hydrogenchloride; water; N,N-dimethyl-formamide; In acetonitrile;

DOI:10.1039/c2ob27004h

upstream raw materials:

3-(2,2-diethoxyethyl)-5-methyl-1,7-diphenyl-2,6-dicarbethoxy-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

3-(2,2-diethoxyethyl)-5-(2-dimethylaminoethen-1-yl)-1,7-diphenyl-2,6-dicarbethoxy-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

3,5-bis(2-acetoxyethen-1-yl)-1,7-diphenyl-2,6-dicarbethoxy-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

aniline