3-O-benzyl-6-O-deoxy-1,2-O-isopropylidene-6-C-(pent-4-enyl)-α-D-allofuranose

Base Information

Chemical Name:3-O-benzyl-6-O-deoxy-1,2-O-isopropylidene-6-C-(pent-4-enyl)-α-D-allofuranose
CAS No.:1257843-89-2
Molecular Formula:C₂₁H₃₀O₅
Molecular Weight:362.466
Hs Code.:

Synonyms:3-O-benzyl-6-O-deoxy-1,2-O-isopropylidene-6-C-(pent-4-enyl)-α-D-allofuranose

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Chemical Property of 3-O-benzyl-6-O-deoxy-1,2-O-isopropylidene-6-C-(pent-4-enyl)-α-D-allofuranose

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Technology Process of 3-O-benzyl-6-O-deoxy-1,2-O-isopropylidene-6-C-(pent-4-enyl)-α-D-allofuranose

There total 1 articles about 3-O-benzyl-6-O-deoxy-1,2-O-isopropylidene-6-C-(pent-4-enyl)-α-D-allofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1119-51-3
bromopentene

: 83103-60-0
5,6-anhydro-3-O-benzyl-1,2-O-isopropylidene-α-D-allofuranose

: 1257843-89-2
3-O-benzyl-6-O-deoxy-1,2-O-isopropylidene-6-C-(pent-4-enyl)-α-D-allofuranose

Guidance literature:: bromopentene; With magnesium; In tetrahydrofuran;

5,6-anhydro-3-O-benzyl-1,2-O-isopropylidene-α-D-allofuranose; With copper(l) iodide; In tetrahydrofuran; at -70 - 20 ℃; for 16h;
DOI:10.1007/s11426-010-4063-3

Reference yield: 84.0%

: 1257843-89-2
3-O-benzyl-6-O-deoxy-1,2-O-isopropylidene-6-C-(pent-4-enyl)-α-D-allofuranose

: 100-39-0
benzyl bromide

: 1257843-90-5
3,5-di-O-benzyl-6-O-deoxy-1,2-O-isopropylidene-6-C-(pent-4-enyl)-α-D-allofuranose

Guidance literature:: 3-O-benzyl-6-O-deoxy-1,2-O-isopropylidene-6-C-(pent-4-enyl)-α-D-allofuranose; With sodium hydride; In tetrahydrofuran; mineral oil; at 20 ℃; for 1h;

benzyl bromide; With tetra-(n-butyl)ammonium iodide; In tetrahydrofuran; mineral oil; at 20 ℃; for 12h;
DOI:10.1007/s11426-010-4063-3