Technology Process of C17H22O5
There total 4 articles about C17H22O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
2,3-Dimethoxy-3'-methyl-butyrophenon;
With
potassium hexamethylsilazane;
In
tetrahydrofuran; toluene;
at -78 ℃;
for 1h;
Inert atmosphere;
Allyl chloroformate;
In
tetrahydrofuran; toluene;
at -78 - 20 ℃;
Inert atmosphere;
DOI:10.1021/ol301332f
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: pyridinium chlorochromate / dichloromethane / 20 °C / Inert atmosphere
2.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 1 h / -78 °C / Inert atmosphere
2.2: -78 - 20 °C / Inert atmosphere
With
potassium hexamethylsilazane; pyridinium chlorochromate;
In
tetrahydrofuran; dichloromethane; toluene;
DOI:10.1021/ol301332f
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine / diethyl ether; hexane / 1 h / 0 - 20 °C / Inert atmosphere
1.2: 0 - 20 °C / Inert atmosphere
2.1: pyridinium chlorochromate / dichloromethane / 20 °C / Inert atmosphere
3.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 1 h / -78 °C / Inert atmosphere
3.2: -78 - 20 °C / Inert atmosphere
With
n-butyllithium; N,N,N,N,-tetramethylethylenediamine; potassium hexamethylsilazane; pyridinium chlorochromate;
In
tetrahydrofuran; diethyl ether; hexane; dichloromethane; toluene;
DOI:10.1021/ol301332f
