2,2'-thio-bis-(4-methyl-(1-oxa-3-oxo-4-aza-6-hydroxyhexyl)-benzene)

Base Information

• Chemical Name: 2,2'-thio-bis-(4-methyl-(1-oxa-3-oxo-4-aza-6-hydroxyhexyl)-benzene)
• CAS No.: 1253641-56-3
• Molecular Formula: C₂₂H₂₈N₂O₆S
• Molecular Weight: 448.54
• Mol file: 1253641-56-3.mol

Synonyms:2,2'-thio-bis-(4-methyl-(1-oxa-3-oxo-4-aza-6-hydroxyhexyl)-benzene)

Chemical Property of 2,2'-thio-bis-(4-methyl-(1-oxa-3-oxo-4-aza-6-hydroxyhexyl)-benzene)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,2'-thio-bis-(4-methyl-(1-oxa-3-oxo-4-aza-6-hydroxyhexyl)-benzene)

There total 2 articles about 2,2'-thio-bis-(4-methyl-(1-oxa-3-oxo-4-aza-6-hydroxyhexyl)-benzene) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

2,2'-sulfinyl bis[methy(4-methylphenoxyacetate)] (882304-68-9) + ethanolamine (141-43-5) → 2,2'-thio-bis-(4-methyl-(1-oxa-3-oxo-4-aza-6-hydroxyhexyl)-benzene) (1253641-56-3)

Guidance literature:

With potassium carbonate; In methanol; at 20 ℃; for 24h;

DOI:10.1080/10426500802417059

Reference yield:

C18H16Cl2O4S (775330-32-0) + ethanolamine (141-43-5) → 2,2'-thio-bis-(4-methyl-(1-oxa-3-oxo-4-aza-6-hydroxyhexyl)-benzene) (1253641-56-3)

Guidance literature:

With triethylamine; In acetonitrile; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1080/10426500802417059

Reference yield: 94.0%

2,2'-thio-bis-(4-methyl-(1-oxa-3-oxo-4-aza-6-hydroxyhexyl)-benzene) (1253641-56-3) → 2,2'-thio-bis-(4-methyl-(1-oxa-3-oxo-4-aza-6-chlorohexyl)-benzene) (1198335-32-8)

Guidance literature:

With thionyl chloride; In chloroform; at 20 ℃; for 4.5h; Reflux;

DOI:10.1080/10426500802417059

upstream raw materials:

2,2'-sulfinyl bis[methy(4-methylphenoxyacetate)]

ethanolamine

C₁₈H₁₆Cl₂O₄S

Downstream raw materials:

2,2'-thio-bis-(4-methyl-(1-oxa-3-oxo-4-aza-6-chlorohexyl)-benzene)