19-methoxy-17-methyl-8-phenylthiomethyl-3,6,10,13-tetraoxabicyclo<13.3.1>nonadeca-1(19),15,17-triene

Base Information

Chemical Name:19-methoxy-17-methyl-8-phenylthiomethyl-3,6,10,13-tetraoxabicyclo<13.3.1>nonadeca-1(19),15,17-triene
CAS No.:122475-96-1
Molecular Formula:C₂₄H₃₂O₅S
Molecular Weight:432.581
Hs Code.:

Synonyms:19-methoxy-17-methyl-8-phenylthiomethyl-3,6,10,13-tetraoxabicyclo<13.3.1>nonadeca-1(19),15,17-triene

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Chemical Property of 19-methoxy-17-methyl-8-phenylthiomethyl-3,6,10,13-tetraoxabicyclo<13.3.1>nonadeca-1(19),15,17-triene

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Technology Process of 19-methoxy-17-methyl-8-phenylthiomethyl-3,6,10,13-tetraoxabicyclo<13.3.1>nonadeca-1(19),15,17-triene

There total 4 articles about 19-methoxy-17-methyl-8-phenylthiomethyl-3,6,10,13-tetraoxabicyclo<13.3.1>nonadeca-1(19),15,17-triene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 108-98-5
thiophenol

: 122475-95-0
19-methoxy-17-methyl-8-methylene-3,6,10,13-tetraoxabicyclo<13.3.1>nonadeca-1(19),15,17-triene

: 122475-96-1
19-methoxy-17-methyl-8-phenylthiomethyl-3,6,10,13-tetraoxabicyclo<13.3.1>nonadeca-1(19),15,17-triene

Guidance literature:: With toluene-4-sulfonic acid; for 12h; Ambient temperature;

Reference yield:

: 6327-85-1
2,6-bis(hydroxymethyl)-4-methyl-anisole

: 122475-96-1
19-methoxy-17-methyl-8-phenylthiomethyl-3,6,10,13-tetraoxabicyclo<13.3.1>nonadeca-1(19),15,17-triene

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / PBr₃ / CH₂Cl₂ / 6 h / Ambient temperature

2: 65 percent / NaH / tetrahydrofuran / 2 h / Heating

3: 74 percent / p-toluenesulfonic acid / 12 h / Ambient temperature

With phosphorus tribromide; sodium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; dichloromethane;

Reference yield:

: 28544-88-9
2,2'-(2-methylenepropane-1,3-diyldioxy)bisethanol

: 122475-96-1
19-methoxy-17-methyl-8-phenylthiomethyl-3,6,10,13-tetraoxabicyclo<13.3.1>nonadeca-1(19),15,17-triene

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / NaH / tetrahydrofuran / 2 h / Heating

2: 74 percent / p-toluenesulfonic acid / 12 h / Ambient temperature

With sodium hydride; toluene-4-sulfonic acid; In tetrahydrofuran;