N-(2-[1-benzyl-1H-1,2,3-triazol-4-yl]propan-2-yl)-3-methyl-[1,1'-biphenyl]-2-carboxamide

Base Information

Chemical Name:N-(2-[1-benzyl-1H-1,2,3-triazol-4-yl]propan-2-yl)-3-methyl-[1,1'-biphenyl]-2-carboxamide
CAS No.:1623775-18-7
Molecular Formula:C₂₆H₂₆N₄O
Molecular Weight:410.519
Hs Code.:

Synonyms:N-(2-[1-benzyl-1H-1,2,3-triazol-4-yl]propan-2-yl)-3-methyl-[1,1'-biphenyl]-2-carboxamide

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Chemical Property of N-(2-[1-benzyl-1H-1,2,3-triazol-4-yl]propan-2-yl)-3-methyl-[1,1'-biphenyl]-2-carboxamide

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Technology Process of N-(2-[1-benzyl-1H-1,2,3-triazol-4-yl]propan-2-yl)-3-methyl-[1,1'-biphenyl]-2-carboxamide

There total 8 articles about N-(2-[1-benzyl-1H-1,2,3-triazol-4-yl]propan-2-yl)-3-methyl-[1,1'-biphenyl]-2-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 591-50-4
iodobenzene

: 1623774-99-1
N-(2-(1-benzyl-1H-1, 2, 3-triazol-4-yl)propan-2-yl)-2-methylbenzamide

: 1623775-18-7
N-(2-[1-benzyl-1H-1,2,3-triazol-4-yl]propan-2-yl)-3-methyl-[1,1'-biphenyl]-2-carboxamide

Guidance literature:: With silver(I) acetate; palladium diacetate; In toluene; at 110 ℃; for 16h; Reagent/catalyst; Temperature; Catalytic behavior; Schlenk technique; Inert atmosphere;
DOI:10.1002/ejoc.201601045

Reference yield: 84.0%

: 108-86-1,52753-63-6
bromobenzene

: 1623774-99-1
N-(2-(1-benzyl-1H-1, 2, 3-triazol-4-yl)propan-2-yl)-2-methylbenzamide

: 1623775-18-7
N-(2-[1-benzyl-1H-1,2,3-triazol-4-yl]propan-2-yl)-3-methyl-[1,1'-biphenyl]-2-carboxamide

Guidance literature:: With tris(triphenylphosphine)ruthenium(II) chloride; sodium carbonate; In o-xylene; at 120 ℃; for 22h; chemoselective reaction; Inert atmosphere; Schlenk technique;
DOI:10.1002/chem.201403019

Reference yield: 82.0%

: 1623774-99-1
N-(2-(1-benzyl-1H-1, 2, 3-triazol-4-yl)propan-2-yl)-2-methylbenzamide

: 100-58-3
phenylmagnesium bromide

: 1623775-18-7
N-(2-[1-benzyl-1H-1,2,3-triazol-4-yl]propan-2-yl)-3-methyl-[1,1'-biphenyl]-2-carboxamide

Guidance literature:: N-(2-(1-benzyl-1H-1, 2, 3-triazol-4-yl)propan-2-yl)-2-methylbenzamide; phenylmagnesium bromide; With iron(III) chloride; N,N,N,N,-tetramethylethylenediamine; zinc dibromide; In tetrahydrofuran; at 20 ℃; for 0.166667h; Inert atmosphere; Schlenk technique;

With 1,2-bis-(diphenylphosphino)ethane; In tetrahydrofuran; at 20 ℃; for 0.166667h;

With 1,2-dichloro-2-methylpropane; In tetrahydrofuran; at 55 ℃; for 36h;
DOI:10.1002/anie.201311024