N-[(3R,5R)-9-(tert-butyldimethylsilyloxy)-5-hydroxy-2-methylnon-6-yn-3-yl]-4-methylphenylsulfonamide

Base Information

Chemical Name:N-[(3R,5R)-9-(tert-butyldimethylsilyloxy)-5-hydroxy-2-methylnon-6-yn-3-yl]-4-methylphenylsulfonamide
CAS No.:1244779-51-8
Molecular Formula:C₂₃H₃₉NO₄SSi
Molecular Weight:453.718
Hs Code.:

Synonyms:N-[(3R,5R)-9-(tert-butyldimethylsilyloxy)-5-hydroxy-2-methylnon-6-yn-3-yl]-4-methylphenylsulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[(3R,5R)-9-(tert-butyldimethylsilyloxy)-5-hydroxy-2-methylnon-6-yn-3-yl]-4-methylphenylsulfonamide

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Technology Process of N-[(3R,5R)-9-(tert-butyldimethylsilyloxy)-5-hydroxy-2-methylnon-6-yn-3-yl]-4-methylphenylsulfonamide

There total 1 articles about N-[(3R,5R)-9-(tert-butyldimethylsilyloxy)-5-hydroxy-2-methylnon-6-yn-3-yl]-4-methylphenylsulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1161012-82-3
(S)-4-methyl-3-tosylamino-1-pentanal

: 78592-82-2
4-(tert-butyldimethylsilyloxy)-1-butyne

: 1244779-52-9
N-[(3R,5S)-9-(tert-butyldimethylsilyloxy)-5-hydroxy-2-methylnon-6-yn-3-yl]-4-methylphenylsulfonamide

: 1244779-51-8
N-[(3R,5R)-9-(tert-butyldimethylsilyloxy)-5-hydroxy-2-methylnon-6-yn-3-yl]-4-methylphenylsulfonamide

Guidance literature:: 4-(tert-butyldimethylsilyloxy)-1-butyne; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 0.166667h; Inert atmosphere;

(S)-4-methyl-3-tosylamino-1-pentanal; In tetrahydrofuran; at -78 ℃; Inert atmosphere;
DOI:10.1002/chem.201000653

Reference yield: 93.0%

: 1244779-51-8
N-[(3R,5R)-9-(tert-butyldimethylsilyloxy)-5-hydroxy-2-methylnon-6-yn-3-yl]-4-methylphenylsulfonamide

: 1244779-62-1
NM-[(3R,5S)-5-bromo-9-(tert-butyldimethylsilyloxy)-2-methylnon-6-yn-3-yl]-4-methylphenylsulfonamide

Guidance literature:: With 1H-imidazole; carbon tetrabromide; triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 2h;
DOI:10.1002/chem.201000653