tert-butyl (S)-3-allyl-5-benzyl-6-(methoxycarbonyl)-14,14-dimethyl-4,12-dioxo-13-oxa-2,3,5,11-tetraazapentadecanoate

Base Information

Chemical Name:tert-butyl (S)-3-allyl-5-benzyl-6-(methoxycarbonyl)-14,14-dimethyl-4,12-dioxo-13-oxa-2,3,5,11-tetraazapentadecanoate
CAS No.:1640012-38-9
Molecular Formula:C₂₈H₄₄N₄O₇
Molecular Weight:548.68
Hs Code.:

Synonyms:tert-butyl (S)-3-allyl-5-benzyl-6-(methoxycarbonyl)-14,14-dimethyl-4,12-dioxo-13-oxa-2,3,5,11-tetraazapentadecanoate

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Chemical Property of tert-butyl (S)-3-allyl-5-benzyl-6-(methoxycarbonyl)-14,14-dimethyl-4,12-dioxo-13-oxa-2,3,5,11-tetraazapentadecanoate

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Technology Process of tert-butyl (S)-3-allyl-5-benzyl-6-(methoxycarbonyl)-14,14-dimethyl-4,12-dioxo-13-oxa-2,3,5,11-tetraazapentadecanoate

There total 5 articles about tert-butyl (S)-3-allyl-5-benzyl-6-(methoxycarbonyl)-14,14-dimethyl-4,12-dioxo-13-oxa-2,3,5,11-tetraazapentadecanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 192725-90-9
tert-butyl 2-(prop-2-en-1-yl)hydrazinecarboxylate

: 32315-10-9
bis(trichloromethyl) carbonate

: 670278-80-5
(S)-methyl 2-(benzylamino)-6-((tert-butoxycarbonyl)amino)hexanoate

: 1640012-38-9
tert-butyl (S)-3-allyl-5-benzyl-6-(methoxycarbonyl)-14,14-dimethyl-4,12-dioxo-13-oxa-2,3,5,11-tetraazapentadecanoate

Guidance literature:: bis(trichloromethyl) carbonate; (S)-methyl 2-(benzylamino)-6-((tert-butoxycarbonyl)amino)hexanoate; With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 20 ℃; for 0.25h; Inert atmosphere;

tert-butyl 2-(prop-2-en-1-yl)hydrazinecarboxylate; In tetrahydrofuran; at 50 ℃; Inert atmosphere;
DOI:10.1039/c6ob01434h

Reference yield:

: 100-52-7
benzaldehyde

: 1640012-38-9
tert-butyl (S)-3-allyl-5-benzyl-6-(methoxycarbonyl)-14,14-dimethyl-4,12-dioxo-13-oxa-2,3,5,11-tetraazapentadecanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / methanol / 1.5 h / 20 °C / Inert atmosphere

2.1: sodium tetrahydroborate / methanol / 0.75 h / 0 - 20 °C / Inert atmosphere

3.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 0.25 h / 20 °C / Inert atmosphere

3.2: 40 °C / Inert atmosphere

With sodium tetrahydroborate; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol;
DOI:10.1039/c4cc03660c

Reference yield:

: 3017-32-1,1372256-52-4
(S)-methyl 2-amino-6-(tert-butoxycarbonylamino)hexanoate

: 1640012-38-9
tert-butyl (S)-3-allyl-5-benzyl-6-(methoxycarbonyl)-14,14-dimethyl-4,12-dioxo-13-oxa-2,3,5,11-tetraazapentadecanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / methanol / 1.5 h / 20 °C / Inert atmosphere

2.1: sodium tetrahydroborate / methanol / 0.75 h / 0 - 20 °C / Inert atmosphere

3.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 0.25 h / 20 °C / Inert atmosphere

3.2: 40 °C / Inert atmosphere

With sodium tetrahydroborate; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol;
DOI:10.1039/c4cc03660c