4-(N-2-acetoxyethyl-N-methylamino)-2-(N-t-butoxycarbonyl-N-methylamino)aniline

Base Information

Chemical Name:4-(N-2-acetoxyethyl-N-methylamino)-2-(N-t-butoxycarbonyl-N-methylamino)aniline
CAS No.:1350439-73-4
Molecular Formula:C₁₇H₂₇N₃O₄
Molecular Weight:337.419
Hs Code.:

Synonyms:4-(N-2-acetoxyethyl-N-methylamino)-2-(N-t-butoxycarbonyl-N-methylamino)aniline

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Chemical Property of 4-(N-2-acetoxyethyl-N-methylamino)-2-(N-t-butoxycarbonyl-N-methylamino)aniline

Chemical Property:

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Technology Process of 4-(N-2-acetoxyethyl-N-methylamino)-2-(N-t-butoxycarbonyl-N-methylamino)aniline

There total 3 articles about 4-(N-2-acetoxyethyl-N-methylamino)-2-(N-t-butoxycarbonyl-N-methylamino)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1350439-71-2
4-(N-2-acetoxyethyl-N-methylamino)-2-(N-t-butoxycarbonyl-N-methylamino)nitrobenzene

: 1350439-73-4
4-(N-2-acetoxyethyl-N-methylamino)-2-(N-t-butoxycarbonyl-N-methylamino)aniline

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; at 20 ℃; for 3h; Inert atmosphere;

Reference yield:

: 1350439-69-8
2-(N-t-butoxycarbonyl-N-methylamino)-4-(N-2-hydroxyethyl-N-methylamino)nitrobenzene

: 1350439-73-4
4-(N-2-acetoxyethyl-N-methylamino)-2-(N-t-butoxycarbonyl-N-methylamino)aniline

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / tetrahydrofuran / 20 °C

2: palladium 10% on activated carbon; hydrogen / methanol / 3 h / 20 °C / Inert atmosphere

With pyridine; palladium 10% on activated carbon; hydrogen; In tetrahydrofuran; methanol;

Reference yield:

: 299176-17-3
N-(2-nitro-5-chlorophenyl)-N-methylcarbamic acid t-butyl ester

: 1350439-73-4
4-(N-2-acetoxyethyl-N-methylamino)-2-(N-t-butoxycarbonyl-N-methylamino)aniline

Guidance literature:: Multi-step reaction with 3 steps

1: 6.5 h / 50 - 110 °C

2: pyridine / tetrahydrofuran / 20 °C

3: palladium 10% on activated carbon; hydrogen / methanol / 3 h / 20 °C / Inert atmosphere

With pyridine; palladium 10% on activated carbon; hydrogen; In tetrahydrofuran; methanol;