Carbamic acid, (5-chloro-2-nitrophenyl)methyl-, 1,1-dimethylethyl ester

Base Information

Chemical Name:Carbamic acid, (5-chloro-2-nitrophenyl)methyl-, 1,1-dimethylethyl ester
CAS No.:299176-17-3
Molecular Formula:C12H15ClN2O4
Molecular Weight:286.715
Hs Code.:
Mol file:299176-17-3.mol

Synonyms:N-t-butoxycarbonyl-N-methyl-5-chloro-2-nitroaniline;

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Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Carbamic acid, (5-chloro-2-nitrophenyl)methyl-, 1,1-dimethylethyl ester

Chemical Property:

PSA：87.64000
LogP:4.00050

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Carbamic acid, (5-chloro-2-nitrophenyl)methyl-, 1,1-dimethylethyl ester

There total 2 articles about Carbamic acid, (5-chloro-2-nitrophenyl)methyl-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.1%

: 24424-99-5
di-tert-butyl dicarbonate

: 35966-84-8
4-chloro-2-methylaminonitrobenzene

: 299176-17-3
N-(2-nitro-5-chlorophenyl)-N-methylcarbamic acid t-butyl ester

Guidance literature:: With dmap; triethylamine; In tetrahydrofuran; at 20 ℃; for 16h;

Reference yield:

: 700-37-8
4-chloro-2-fluoro-nitrobenzene

: 299176-17-3
N-(2-nitro-5-chlorophenyl)-N-methylcarbamic acid t-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol / 2.25 h / 0 °C

2: dmap; triethylamine / tetrahydrofuran / 16 h / 20 °C

With dmap; triethylamine; In tetrahydrofuran; ethanol;