(1S,3R,4aR,7R,8S,8aR)-8-[(tert-butyldiphenylsiloxy)methyl]tetrahydro-1,3-dihydroxy-8a-[3-(methoxymethoxy)propyl]-3,4,4,7-tetramethyl-6(5H)-isochromanone

Base Information

Chemical Name:(1S,3R,4aR,7R,8S,8aR)-8-[(tert-butyldiphenylsiloxy)methyl]tetrahydro-1,3-dihydroxy-8a-[3-(methoxymethoxy)propyl]-3,4,4,7-tetramethyl-6(5H)-isochromanone
CAS No.:607405-75-4
Molecular Formula:C₃₅H₅₂O₇Si
Molecular Weight:612.879
Hs Code.:

(1S,3R,4aR,7R,8S,8aR)-8-[(tert-butyldiphenylsiloxy)methyl]tetrahydro-1,3-dihydroxy-8a-[3-(methoxymethoxy)propyl]-3,4,4,7-tetramethyl-6(5H)-isochromanone

Synonyms:(1S,3R,4aR,7R,8S,8aR)-8-[(tert-butyldiphenylsiloxy)methyl]tetrahydro-1,3-dihydroxy-8a-[3-(methoxymethoxy)propyl]-3,4,4,7-tetramethyl-6(5H)-isochromanone

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Chemical Property of (1S,3R,4aR,7R,8S,8aR)-8-[(tert-butyldiphenylsiloxy)methyl]tetrahydro-1,3-dihydroxy-8a-[3-(methoxymethoxy)propyl]-3,4,4,7-tetramethyl-6(5H)-isochromanone

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Technology Process of (1S,3R,4aR,7R,8S,8aR)-8-[(tert-butyldiphenylsiloxy)methyl]tetrahydro-1,3-dihydroxy-8a-[3-(methoxymethoxy)propyl]-3,4,4,7-tetramethyl-6(5H)-isochromanone

There total 1 articles about (1S,3R,4aR,7R,8S,8aR)-8-[(tert-butyldiphenylsiloxy)methyl]tetrahydro-1,3-dihydroxy-8a-[3-(methoxymethoxy)propyl]-3,4,4,7-tetramethyl-6(5H)-isochromanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 607405-74-3
(3aR,6R,7S,7aR)-7-[(tert-butyldiphenylsilyloxy)methyl]-3,3a,4,6,7,7a-hexahydro-7a-[3-(methoxymethoxy)propyl]-2,3,3,6-tetramethyl-5H-inden-5-one

: 607405-75-4
(1S,3R,4aR,7R,8S,8aR)-8-[(tert-butyldiphenylsiloxy)methyl]tetrahydro-1,3-dihydroxy-8a-[3-(methoxymethoxy)propyl]-3,4,4,7-tetramethyl-6(5H)-isochromanone

Guidance literature:: (3aR,6R,7S,7aR)-7-[(tert-butyldiphenylsilyloxy)methyl]-3,3a,4,6,7,7a-hexahydro-7a-[3-(methoxymethoxy)propyl]-2,3,3,6-tetramethyl-5H-inden-5-one; With pyridine; ozone; In methanol; dichloromethane; at -78 ℃;

With dimethylsulfide; In methanol; dichloromethane; at -78 - 20 ℃;
DOI:10.1021/jo0301346