ethy{[6-(4-chlorophenyl)-3-cyano-4-(2-furyl)pyridine-2-yl]-thio}acetate

Base Information

Chemical Name:ethy{[6-(4-chlorophenyl)-3-cyano-4-(2-furyl)pyridine-2-yl]-thio}acetate
CAS No.:1334548-47-8
Molecular Formula:C₂₀H₁₅ClN₂O₃S
Molecular Weight:398.87
Hs Code.:

Synonyms:ethy{[6-(4-chlorophenyl)-3-cyano-4-(2-furyl)pyridine-2-yl]-thio}acetate

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Chemical Property of ethy{[6-(4-chlorophenyl)-3-cyano-4-(2-furyl)pyridine-2-yl]-thio}acetate

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Technology Process of ethy{[6-(4-chlorophenyl)-3-cyano-4-(2-furyl)pyridine-2-yl]-thio}acetate

There total 2 articles about ethy{[6-(4-chlorophenyl)-3-cyano-4-(2-furyl)pyridine-2-yl]-thio}acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1334548-45-6
6-(4-chlorophenyl)-4-(2-furyl)-2-thioxo-1,2-dihydropyridine-3-carbonitrile

: 105-36-2
ethyl bromoacetate

: 1334548-47-8
ethy{[6-(4-chlorophenyl)-3-cyano-4-(2-furyl)pyridine-2-yl]-thio}acetate

Guidance literature:: 6-(4-chlorophenyl)-4-(2-furyl)-2-thioxo-1,2-dihydropyridine-3-carbonitrile; With potassium hydroxide; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

ethyl bromoacetate; In N,N-dimethyl-formamide; at 20 ℃; for 2h;
DOI:10.1080/17415993.2011.593635

Reference yield:

: 14385-65-0,114570-70-6
(2E)-1-(4-chlorophenyl)-3-(2-furyl)prop-2-en-1-one

: 1334548-47-8
ethy{[6-(4-chlorophenyl)-3-cyano-4-(2-furyl)pyridine-2-yl]-thio}acetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium ethanolate / ethanol / 4 h / Reflux

2.1: potassium hydroxide / N,N-dimethyl-formamide / 2 h / 20 °C

2.2: 2 h / 20 °C

With sodium ethanolate; potassium hydroxide; In ethanol; N,N-dimethyl-formamide;
DOI:10.1080/17415993.2011.593635