O-(4-methoxyphenyl)-N,N-diethylthiocarbamate

Base Information

Chemical Name:O-(4-methoxyphenyl)-N,N-diethylthiocarbamate
CAS No.:191607-97-3
Molecular Formula:C₁₂H₁₇NO₂S
Molecular Weight:239.338
Hs Code.:

Synonyms:O-(4-methoxyphenyl)-N,N-diethylthiocarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of O-(4-methoxyphenyl)-N,N-diethylthiocarbamate

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Technology Process of O-(4-methoxyphenyl)-N,N-diethylthiocarbamate

There total 1 articles about O-(4-methoxyphenyl)-N,N-diethylthiocarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 88-11-9
N,N-diethylthiocarbamoyl chloride

: 150-76-5
4-methoxy-phenol

: 191607-97-3
O-(4-methoxyphenyl)-N,N-diethylthiocarbamate

Guidance literature:: With dmap; triethylamine; In 1,4-dioxane; for 18h; Heating;
DOI:10.1080/00397919708004112

Reference yield:

: 7311-34-4
3,5-dimethoxybenzaldehdye

: 191607-97-3
O-(4-methoxyphenyl)-N,N-diethylthiocarbamate

: 705-76-0
3,5-dimethoxybenzyl alcohol

: O-[2-(3',5'-dimethoxy-α-hydroxybenzyl)-4-methoxyphenyl] N,N-diethylthiocarbamate

: O-[3-(3',5'-dimethoxy-α-hydroxybenzyl)-4-methoxyphenyl] N,N-diethylthiocarbamate

Guidance literature:: With N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; Yield given. Multistep reaction. Yields of byproduct given; 1) cyclohexane, THF, -78 deg C, 2 h; 2) cyclohexane, THF, -78 deg C, 1 h;
DOI:10.1080/00397919708004112

Reference yield:

: 88-10-8
N,N-diethylcarbamyl chloride

: 191607-97-3
O-(4-methoxyphenyl)-N,N-diethylthiocarbamate

: O-(2-N,N-diethylcarboxamido-4-methoxyphenyl)-N,N-diethylthicarbamate

: O-(3-N,N-diethylcarboxamido-4-methoxyphenyl)-N,N-diethylthicarbamate

Guidance literature:: With N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; Yield given. Multistep reaction. Yields of byproduct given; 1) cyclohexane, THF, -78 deg C, 2 h; 2) cyclohexane, THF, -78 deg C, 1 h;
DOI:10.1080/00397919708004112