Technology Process of C34H50O7Si
There total 13 articles about C34H50O7Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dmap; dicyclohexyl-carbodiimide;
In
dichloromethane;
at 20 ℃;
Inert atmosphere;
DOI:10.1002/ejoc.201201338
- Guidance literature:
-
Multi-step reaction with 6 steps
1: AD-mix-β; methanesulfonamide; water / tert-butyl alcohol / 48 h / 0 °C / Inert atmosphere
2: toluene-4-sulfonic acid / acetone / 20 °C / Inert atmosphere
3: tetrabutyl ammonium fluoride / tetrahydrofuran / 5 h / 20 °C / Inert atmosphere
4: Dess-Martin periodane / dichloromethane / 1.5 h / 20 °C / Inert atmosphere
5: sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene; sodium chlorite / water; tetrahydrofuran; tert-butyl alcohol / 20 °C / Inert atmosphere
6: dicyclohexyl-carbodiimide; dmap / dichloromethane / 20 °C / Inert atmosphere
With
dmap; sodium chlorite; sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene; methanesulfonamide; AD-mix-β; tetrabutyl ammonium fluoride; water; Dess-Martin periodane; toluene-4-sulfonic acid; dicyclohexyl-carbodiimide;
In
tetrahydrofuran; dichloromethane; water; acetone; tert-butyl alcohol;
DOI:10.1002/ejoc.201201338
- Guidance literature:
-
Multi-step reaction with 5 steps
1: toluene-4-sulfonic acid / acetone / 20 °C / Inert atmosphere
2: tetrabutyl ammonium fluoride / tetrahydrofuran / 5 h / 20 °C / Inert atmosphere
3: Dess-Martin periodane / dichloromethane / 1.5 h / 20 °C / Inert atmosphere
4: sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene; sodium chlorite / water; tetrahydrofuran; tert-butyl alcohol / 20 °C / Inert atmosphere
5: dicyclohexyl-carbodiimide; dmap / dichloromethane / 20 °C / Inert atmosphere
With
dmap; sodium chlorite; sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene; tetrabutyl ammonium fluoride; Dess-Martin periodane; toluene-4-sulfonic acid; dicyclohexyl-carbodiimide;
In
tetrahydrofuran; dichloromethane; water; acetone; tert-butyl alcohol;
DOI:10.1002/ejoc.201201338