tert-butyl diphenyl(2-((4R,5R)-2,2,5-trimethyl-1,3-dioxolan-4-yl)ethoxy)silane

Base Information

Chemical Name:tert-butyl diphenyl(2-((4R,5R)-2,2,5-trimethyl-1,3-dioxolan-4-yl)ethoxy)silane
CAS No.:1449467-80-4
Molecular Formula:C₂₄H₃₄O₃Si
Molecular Weight:398.618
Hs Code.:

Synonyms:tert-butyl diphenyl(2-((4R,5R)-2,2,5-trimethyl-1,3-dioxolan-4-yl)ethoxy)silane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl diphenyl(2-((4R,5R)-2,2,5-trimethyl-1,3-dioxolan-4-yl)ethoxy)silane

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Technology Process of tert-butyl diphenyl(2-((4R,5R)-2,2,5-trimethyl-1,3-dioxolan-4-yl)ethoxy)silane

There total 4 articles about tert-butyl diphenyl(2-((4R,5R)-2,2,5-trimethyl-1,3-dioxolan-4-yl)ethoxy)silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1449467-79-1
(2R,3R)-5-(tert-butyl diphenylsilyloxy)pentane-2,3-diol

: 77-76-9
2,2-dimethoxy-propane

: 1449467-80-4
tert-butyl diphenyl(2-((4R,5R)-2,2,5-trimethyl-1,3-dioxolan-4-yl)ethoxy)silane

Guidance literature:: With toluene-4-sulfonic acid; In water; acetone; at 20 ℃;

Reference yield:

: 764-37-4
(E)-3-penten-1-ol

: 1449467-80-4
tert-butyl diphenyl(2-((4R,5R)-2,2,5-trimethyl-1,3-dioxolan-4-yl)ethoxy)silane

Guidance literature:: Multi-step reaction with 3 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

2: AD-mix-β; methanesulfonamide; water / tert-butyl alcohol / 48 h / 0 °C / Inert atmosphere

3: toluene-4-sulfonic acid / acetone / 20 °C / Inert atmosphere

With 1H-imidazole; methanesulfonamide; AD-mix-β; water; toluene-4-sulfonic acid; In N,N-dimethyl-formamide; acetone; tert-butyl alcohol;
DOI:10.1002/ejoc.201201338

Reference yield:

: 124070-55-9
(E)-tert-butyl (pent-3-enyloxy)diphenylsilane

: 1449467-80-4
tert-butyl diphenyl(2-((4R,5R)-2,2,5-trimethyl-1,3-dioxolan-4-yl)ethoxy)silane

Guidance literature:: Multi-step reaction with 2 steps

1: methanesulfonamide; (DHQD)₂PHAL / water; tert-butyl alcohol / 48 h / 0 °C

2: toluene-4-sulfonic acid / water; acetone / 20 °C

With methanesulfonamide; (DHQD)₂PHAL; toluene-4-sulfonic acid; In water; acetone; tert-butyl alcohol;