N-[(2-but-2-enylphenyl)acetyl]-2-(ethylsulfanyl)-N-(4-methoxybenzyl)acetamide

Base Information

Chemical Name:N-[(2-but-2-enylphenyl)acetyl]-2-(ethylsulfanyl)-N-(4-methoxybenzyl)acetamide
CAS No.:269405-46-1
Molecular Formula:C₂₄H₂₉NO₃S
Molecular Weight:411.565
Hs Code.:

Synonyms:N-[(2-but-2-enylphenyl)acetyl]-2-(ethylsulfanyl)-N-(4-methoxybenzyl)acetamide

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Chemical Property of N-[(2-but-2-enylphenyl)acetyl]-2-(ethylsulfanyl)-N-(4-methoxybenzyl)acetamide

Chemical Property:

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Technology Process of N-[(2-but-2-enylphenyl)acetyl]-2-(ethylsulfanyl)-N-(4-methoxybenzyl)acetamide

There total 5 articles about N-[(2-but-2-enylphenyl)acetyl]-2-(ethylsulfanyl)-N-(4-methoxybenzyl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 54256-37-0
2-(ethylthio)acetyl chloride

: 269405-44-9
(E)-2-(but-2-enyl-phenyl)-N-(4-methoxybenzyl)acetamide

: 269405-46-1
N-[(2-but-2-enylphenyl)acetyl]-2-(ethylsulfanyl)-N-(4-methoxybenzyl)acetamide

Guidance literature:: In benzene; for 12h; Heating;
DOI:10.1021/jo9915729

Reference yield:

: 82316-08-3,560134-60-3
2-((E)-but-2-en-1-yl)benzyl alcohol

: 269405-46-1
N-[(2-but-2-enylphenyl)acetyl]-2-(ethylsulfanyl)-N-(4-methoxybenzyl)acetamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: 76 percent / PBr₃; pyridine / benzene / 0.17 h / 0 °C

2.1: 94 percent / dimethylsulfoxide / 0.33 h / 20 °C

3.1: 93 percent / KOH / aq. ethanol / 15 h / Heating

4.1: oxalyl chloride / benzene; dimethylformamide / 2 h

4.2: 87 percent / CH₂Cl₂ / 0.33 h / 20 °C

5.1: 87 percent / benzene / 12 h / Heating

With pyridine; potassium hydroxide; oxalyl dichloride; phosphorus tribromide; In ethanol; dimethyl sulfoxide; N,N-dimethyl-formamide; benzene; 1.1: Bromination / 2.1: Substitution / 3.1: Hydrolysis / 4.1: Substitution / 4.2: Acylation / 5.1: Acylation;
DOI:10.1021/jo9915729

Reference yield:

: 269405-43-8
(E)-1-(bromomethyl)-2-but-2-enylbenzene

: 269405-46-1
N-[(2-but-2-enylphenyl)acetyl]-2-(ethylsulfanyl)-N-(4-methoxybenzyl)acetamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: 94 percent / dimethylsulfoxide / 0.33 h / 20 °C

2.1: 93 percent / KOH / aq. ethanol / 15 h / Heating

3.1: oxalyl chloride / benzene; dimethylformamide / 2 h

3.2: 87 percent / CH₂Cl₂ / 0.33 h / 20 °C

4.1: 87 percent / benzene / 12 h / Heating

With potassium hydroxide; oxalyl dichloride; In ethanol; dimethyl sulfoxide; N,N-dimethyl-formamide; benzene; 1.1: Substitution / 2.1: Hydrolysis / 3.1: Substitution / 3.2: Acylation / 4.1: Acylation;
DOI:10.1021/jo9915729