Phosphorane,tetrachloro(trifluoromethyl)-, (TB-5-12)- (9CI)

Base Information

• Chemical Name: Phosphorane,tetrachloro(trifluoromethyl)-, (TB-5-12)- (9CI)
• CAS No.: 1066-48-4
• Molecular Formula: CCl4 F3 P
• Molecular Weight: 241.792
• Mol file: 1066-48-4.mol

Synonyms:Phosphorane,tetrachloro(trifluoromethyl)- (6CI,7CI,8CI);Tetrachloro(trifluoromethyl)phosphorane

Chemical Property of Phosphorane,tetrachloro(trifluoromethyl)-, (TB-5-12)- (9CI)

Chemical Property:

• Boiling Point: 104 °C
• PSA: 13.59000
• LogP: 4.67470

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s): 3
• Hazard Codes: 3:
• Safety Statements: Explosive reaction with tetramethyllead. When hea"> −, F−, and POx. See also CHLORIDES and FLUORIDES." target="_blank">Explosive reaction with tetramethyllead. When hea

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Phosphorane,tetrachloro(trifluoromethyl)-, (TB-5-12)- (9CI)

There total 9 articles about Phosphorane,tetrachloro(trifluoromethyl)-, (TB-5-12)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Tetrakis(trifluoromethyl)cyclotetraphosphane (393-02-2) → Trifluormethyl-tetrachlor-phosphoran (1066-48-4)

Guidance literature:

With chlorine; In neat (no solvent); heating Cl2 in excess with tetramer from 190°C to ambient temp.;;

Reference yield:

pentakis-trifluoromethyl-cyclopentaphosphane (745-23-3,54548-49-1) → Trifluormethyl-tetrachlor-phosphoran (1066-48-4)

Guidance literature:

With chlorine; In neat (no solvent); heating Cl2 in excess with pentamer from 190°C to ambient temp.;;

Reference yield:

(trifluoromethyl)phosphonous dichloride (421-58-9) → Trifluormethyl-tetrachlorphosphoran (1066-48-4)

Guidance literature:

chlorination;

upstream raw materials:

Tetrakis(trifluoromethyl)cyclotetraphosphane

chlorine

pentakis-trifluoromethyl-cyclopentaphosphane

(trifluoromethyl)phosphonous dichloride

Downstream raw materials:

chlorotrifluoromethane

(trifluoromethyl)phosphonous dichloride

phosphorus pentachloride

CF₃P{N(CH₃)2}3⁽¹⁺⁾*Cl^(1-)