Technology Process of 1,6-di-O-benzoyl-3-deoxy-4,5-O-isopropylidene-3-C-methyl-2-O-methyl-L-altritol
There total 7 articles about 1,6-di-O-benzoyl-3-deoxy-4,5-O-isopropylidene-3-C-methyl-2-O-methyl-L-altritol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pyridine;
for 1h;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 80 percent / toluene-p-sulfonic acid-mono hydrate / methanol / 5 h / 0 °C
2: 76 percent / H2 / Raney-Ni / ethanol / 18 h / Ambient temperature
3: sodium periodate / acetone / 4 h / 0 °C / pH 6-7
4: sodium borohydride / methanol / 2 h / 0 °C
5: 96 percent / pyridine / 1 h / Ambient temperature
With
pyridine; sodium tetrahydroborate; sodium periodate; hydrogen; toluene-4-sulfonic acid;
nickel;
In
methanol; ethanol; acetone;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 2.) KH / 1.) THF, Et2O, RT, 3 h, 2.) THF, RT, 30 min
2: 80 percent / toluene-p-sulfonic acid-mono hydrate / methanol / 5 h / 0 °C
3: 76 percent / H2 / Raney-Ni / ethanol / 18 h / Ambient temperature
4: sodium periodate / acetone / 4 h / 0 °C / pH 6-7
5: sodium borohydride / methanol / 2 h / 0 °C
6: 96 percent / pyridine / 1 h / Ambient temperature
With
pyridine; sodium tetrahydroborate; sodium periodate; hydrogen; potassium hydride; toluene-4-sulfonic acid;
nickel;
In
methanol; ethanol; acetone;
