2-(2,6-diethylphenyl)-N-(3-(3-sulfamoylphenyl)-1H-indazol-5-yl)acetamide

Base Information

Chemical Name:2-(2,6-diethylphenyl)-N-(3-(3-sulfamoylphenyl)-1H-indazol-5-yl)acetamide
CAS No.:1338792-70-3
Molecular Formula:C₂₅H₂₆N₄O₃S
Molecular Weight:462.572
Hs Code.:

Synonyms:2-(2,6-diethylphenyl)-N-(3-(3-sulfamoylphenyl)-1H-indazol-5-yl)acetamide

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Chemical Property of 2-(2,6-diethylphenyl)-N-(3-(3-sulfamoylphenyl)-1H-indazol-5-yl)acetamide

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Technology Process of 2-(2,6-diethylphenyl)-N-(3-(3-sulfamoylphenyl)-1H-indazol-5-yl)acetamide

There total 8 articles about 2-(2,6-diethylphenyl)-N-(3-(3-sulfamoylphenyl)-1H-indazol-5-yl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 23.0%

: 3-(5-amino-1H-indazol-3-yl)benzenesulfonamide 2,2,2-trifluoroacetate

: 100256-33-5
2-(2,6-diethylphenyl)acetic acid

: 1338792-70-3
2-(2,6-diethylphenyl)-N-(3-(3-sulfamoylphenyl)-1H-indazol-5-yl)acetamide

Guidance literature:: With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 0 - 20 ℃;
DOI:10.1016/j.bmc.2014.06.027

Reference yield: 23.0%

: 1338792-70-3
2-(2,6-diethylphenyl)-N-(3-(3-sulfamoylphenyl)-1H-indazol-5-yl)acetamide

Guidance literature:

Reference yield:

: 65232-57-7
1,3-diethyl-2-bromobenzene

: 1338792-70-3
2-(2,6-diethylphenyl)-N-(3-(3-sulfamoylphenyl)-1H-indazol-5-yl)acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: bis(dibenzylideneacetone)-palladium⁽⁰⁾; 1,3-bis[2,6-diisopropylphenyl]imidazolium chloride; lithium hexamethyldisilazane / toluene; hexane / 16 h / 20 °C / Sealed tube; Inert atmosphere

2: triethylsilane; trifluoroacetic acid / dichloromethane / 3 h / 0 °C

3: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0 - 20 °C

With triethylsilane; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; lithium hexamethyldisilazane; bis(dibenzylideneacetone)-palladium⁽⁰⁾; 1,3-bis[2,6-diisopropylphenyl]imidazolium chloride; In hexane; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.bmc.2014.06.027