(S)-2-(tert-Butyldiphenylsilyl)-3-(p-tolylsulfonyloxy)propanal diethyl acetal

Base Information

Chemical Name:(S)-2-(tert-Butyldiphenylsilyl)-3-(p-tolylsulfonyloxy)propanal diethyl acetal
CAS No.:162893-09-6
Molecular Formula:C₃₀H₄₀O₆SSi
Molecular Weight:556.796
Hs Code.:

Synonyms:(S)-2-(tert-Butyldiphenylsilyl)-3-(p-tolylsulfonyloxy)propanal diethyl acetal

Suppliers and Price of (S)-2-(tert-Butyldiphenylsilyl)-3-(p-tolylsulfonyloxy)propanal diethyl acetal

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (S)-2-(tert-Butyldiphenylsilyl)-3-(p-tolylsulfonyloxy)propanal diethyl acetal

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (S)-2-(tert-Butyldiphenylsilyl)-3-(p-tolylsulfonyloxy)propanal diethyl acetal

There total 3 articles about (S)-2-(tert-Butyldiphenylsilyl)-3-(p-tolylsulfonyloxy)propanal diethyl acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 58479-61-1
tert-butylchlorodiphenylsilane

: 162893-08-5
(S)-2-Hydroxy-3-(p-tolylsulfonyloxy)propanal diethyl acetal

: 162893-09-6
(S)-2-(tert-Butyldiphenylsilyl)-3-(p-tolylsulfonyloxy)propanal diethyl acetal

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; Ambient temperature;
DOI:10.1002/recl.19951140107

Reference yield:

: 142169-24-2
3-(1S-hydroxy-2-(p-toluenesulfonyl)oxyethyl)-1,5-dihydro-3H-2,4-benzodioxepine

: 162893-09-6
(S)-2-(tert-Butyldiphenylsilyl)-3-(p-tolylsulfonyloxy)propanal diethyl acetal

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / 10percentPd/C / ethanol

2: TFA / ethanol / 1.5 h

3: 94 percent / imidazole / dimethylformamide / Ambient temperature

With 1H-imidazole; hydrogen; trifluoroacetic acid; 10% palladium on active carbon; In ethanol; N,N-dimethyl-formamide;
DOI:10.1002/recl.19951140107

Reference yield:

: Toluene-4-sulfonic acid (S)-2-hydroxy-3-oxo-propyl ester

: 162893-09-6
(S)-2-(tert-Butyldiphenylsilyl)-3-(p-tolylsulfonyloxy)propanal diethyl acetal

Guidance literature:: Multi-step reaction with 2 steps

1: TFA / ethanol / 1.5 h

2: 94 percent / imidazole / dimethylformamide / Ambient temperature

With 1H-imidazole; trifluoroacetic acid; In ethanol; N,N-dimethyl-formamide;
DOI:10.1002/recl.19951140107