C₁₄H₁₆NO⁽¹⁺⁾*Br^(1-)

Base Information

• Chemical Name: C₁₄H₁₆NO⁽¹⁺⁾*Br^(1-)
• CAS No.: 1443118-00-0
• Molecular Formula: Br*C₁₄H₁₆NO
• Molecular Weight: 294.191
• Mol file: 1443118-00-0.mol

Synonyms:C₁₄H₁₆NO⁽¹⁺⁾*Br^(1-)

Chemical Property of C₁₄H₁₆NO⁽¹⁺⁾*Br^(1-)

Chemical Property:

Purity/Quality:

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Technology Process of C₁₄H₁₆NO⁽¹⁺⁾*Br^(1-)

There total 1 articles about C₁₄H₁₆NO⁽¹⁺⁾*Br^(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

rac-1-(pyridin-4-yl)ethanol (23389-75-5,42732-22-9) + benzyl bromide (100-39-0) → C14H16NO(1+)*Br(1-) (1443118-00-0)

Guidance literature:

In acetonitrile; at 85 ℃; for 0.25h; Reflux;

DOI:10.1002/adsc.201201034

Reference yield: 81.0%

C14H16NO(1+)*Br(1-) (1443118-00-0) → 1-(1-benzyl-1,2,3,6-tetrahydropyridin-4-yl)ethanol

Guidance literature:

With bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; triethylammonium formate; potassium iodide; In dichloromethane; at 40 ℃; for 24h; chemoselective reaction; Sealed tube;

DOI:10.1002/adsc.201201034

upstream raw materials:

rac-1-(pyridin-4-yl)ethanol

benzyl bromide