diethyl 2-[3,5-dichloro-4-(3'-iso-propyl-4'-methoxyphenoxy)]-2-oxoethylphosphonate

Base Information

Chemical Name:diethyl 2-[3,5-dichloro-4-(3'-iso-propyl-4'-methoxyphenoxy)]-2-oxoethylphosphonate
CAS No.:852948-61-9
Molecular Formula:C₂₂H₂₇Cl₂O₆P
Molecular Weight:489.333
Hs Code.:

Synonyms:diethyl 2-[3,5-dichloro-4-(3'-iso-propyl-4'-methoxyphenoxy)]-2-oxoethylphosphonate

Suppliers and Price of diethyl 2-[3,5-dichloro-4-(3'-iso-propyl-4'-methoxyphenoxy)]-2-oxoethylphosphonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of diethyl 2-[3,5-dichloro-4-(3'-iso-propyl-4'-methoxyphenoxy)]-2-oxoethylphosphonate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of diethyl 2-[3,5-dichloro-4-(3'-iso-propyl-4'-methoxyphenoxy)]-2-oxoethylphosphonate

There total 2 articles about diethyl 2-[3,5-dichloro-4-(3'-iso-propyl-4'-methoxyphenoxy)]-2-oxoethylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 683-08-9
Diethyl methylphosphonate

: 219692-18-9
methyl 3,5-dichloro-4-(4-methoxy-3-isopropylphenoxy)benzoate

: 852948-61-9
diethyl 2-[3,5-dichloro-4-(3'-iso-propyl-4'-methoxyphenoxy)]-2-oxoethylphosphonate

Guidance literature:: Diethyl methylphosphonate; With n-butyllithium; In tetrahydrofuran; hexanes; at -78 ℃; for 1h;

methyl 3,5-dichloro-4-(4-methoxy-3-isopropylphenoxy)benzoate; In tetrahydrofuran; hexanes; at -78 ℃; for 1h;

Reference yield:

: bis(3-isopropyl-4-methoxyphenyl)iodonium tetrafluoroborate

: 852948-61-9
diethyl 2-[3,5-dichloro-4-(3'-iso-propyl-4'-methoxyphenoxy)]-2-oxoethylphosphonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: copper; triethylamine / dichloromethane / 72 h / 0 - 20 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C

2.2: 1 h / -78 °C

With n-butyllithium; copper; triethylamine; In tetrahydrofuran; hexane; dichloromethane;

Reference yield: 83.0%

: 852948-61-9
diethyl 2-[3,5-dichloro-4-(3'-iso-propyl-4'-methoxyphenoxy)]-2-oxoethylphosphonate

: 852948-63-1
2-[3,5-dichloro-4-(3'-iso-propyl-4'-methoxyphenoxy)phenyl]-2-oxoethylphosphonic acid

Guidance literature:: diethyl 2-[3,5-dichloro-4-(3'-iso-propyl-4'-methoxyphenoxy)]-2-oxoethylphosphonate; With trimethylsilyl bromide; In dichloromethane; at 0 - 20 ℃; for 16.5h;

With methanol;