PhClSi[(CH2)2MePhSi(η5-C5H4)Fe(η5-C5H5)]2

Base Information

Chemical Name:PhClSi[(CH2)2MePhSi(η5-C5H4)Fe(η5-C5H5)]2
CAS No.:956029-31-5
Molecular Formula:C₄₄H₄₇ClFe₂Si₃
Molecular Weight:807.261
Hs Code.:

Synonyms:PhClSi[(CH2)2MePhSi(η5-C5H4)Fe(η5-C5H5)]2

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Chemical Property of PhClSi[(CH2)2MePhSi(η5-C5H4)Fe(η5-C5H5)]2

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Technology Process of PhClSi[(CH2)2MePhSi(η5-C5H4)Fe(η5-C5H5)]2

There total 1 articles about PhClSi[(CH2)2MePhSi(η5-C5H4)Fe(η5-C5H5)]2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: ferrocenylmethylphenylvinylsilane

: 4206-75-1
phenylchlorosilane

: 956029-31-5
PhClSi[(CH2)2MePhSi(η5-C5H4)Fe(η5-C5H5)]2

Guidance literature:: platinum 1,3-divinyl-1,1,3,3-tetramethyldisiloxane; In toluene; (Ar); std. Schlenk technique; Pt catalyst was added to soln. of Fe complex in toluene; mixt. was stirred at room temp. for 0.5 h; soln. of silane in toluene was added dropwise; heated at 40°C for few min; IR and NMR monitoring; filtered; solvent removed (vac.);
DOI:10.1021/om700559t

Reference yield: 57.0%

: 956029-31-5
PhClSi[(CH2)2MePhSi(η5-C5H4)Fe(η5-C5H5)]2

: 1730-25-2
allylmagnesium bromide

: 956029-32-6
(CH2=CHCH2)PhSi[(CH2)2MePhSi(η5-C5H4)Fe(η5-C5H5)]2

Guidance literature:: In diethyl ether; (Ar); std. Schlenk technique; soln. of Fe complex in Et2O was added dropwise with stirring to soln. of Mg compd. in Et2O; refluxed for 4 h; cooled to 0°C; aq. NH4Cl added; org. layer septd.; washed (H2O); dried (MgSO4); solvent removed (vac.); chromd. (silica gel, hexane); solvent removed (vac.); elem. anal.;
DOI:10.1021/om700559t