2-Trimethylsilanyl-ethanesulfonic acid [(R)-1-(2-benzenesulfonyl-ethyl)-decyl]-amide

Base Information

Chemical Name:2-Trimethylsilanyl-ethanesulfonic acid [(R)-1-(2-benzenesulfonyl-ethyl)-decyl]-amide
CAS No.:382653-93-2
Molecular Formula:C₂₃H₄₃NO₄S₂Si
Molecular Weight:489.816
Hs Code.:

Synonyms:2-Trimethylsilanyl-ethanesulfonic acid [(R)-1-(2-benzenesulfonyl-ethyl)-decyl]-amide

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Chemical Property of 2-Trimethylsilanyl-ethanesulfonic acid [(R)-1-(2-benzenesulfonyl-ethyl)-decyl]-amide

Chemical Property:

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Technology Process of 2-Trimethylsilanyl-ethanesulfonic acid [(R)-1-(2-benzenesulfonyl-ethyl)-decyl]-amide

There total 7 articles about 2-Trimethylsilanyl-ethanesulfonic acid [(R)-1-(2-benzenesulfonyl-ethyl)-decyl]-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 3112-85-4
methylphenylsulfonate

: 382653-94-3
(R)-2-Nonyl-1-(2-trimethylsilanyl-ethanesulfonyl)-aziridine

: 382653-93-2
2-Trimethylsilanyl-ethanesulfonic acid [(R)-1-(2-benzenesulfonyl-ethyl)-decyl]-amide

Guidance literature:: methylphenylsulfonate; With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In tetrahydrofuran; at -78 ℃;

(R)-2-Nonyl-1-(2-trimethylsilanyl-ethanesulfonyl)-aziridine; In tetrahydrofuran; at -78 - 20 ℃;
DOI:10.1055/s-2001-17440

Reference yield:

: 382653-95-4
N-(1-hydroxymethyl-2-oxo-decyl)-4-methyl-benzenesulfonamide

: 382653-93-2
2-Trimethylsilanyl-ethanesulfonic acid [(R)-1-(2-benzenesulfonyl-ethyl)-decyl]-amide

Guidance literature:: Multi-step reaction with 6 steps

1.1: BF₃*OEt₂ / CH₂Cl₂

2.1: ethanol / Raney nickel / Heating

3.1: 91 percent / KOH; TsCl / tetrahydrofuran / 20 °C

4.1: Na; naphthalene / tetrahydrofuran / -78 °C

5.1: DMAP; Et₃N / CH₂Cl₂ / 0 °C

6.1: n-BuLi; TMEDA / tetrahydrofuran / -78 °C

6.2: 89 percent / tetrahydrofuran / -78 - 20 °C

With dmap; potassium hydroxide; n-butyllithium; naphthalene; ethanol; N,N,N,N,-tetramethylethylenediamine; boron trifluoride diethyl etherate; sodium; triethylamine; p-toluenesulfonyl chloride; nickel; In tetrahydrofuran; dichloromethane;
DOI:10.1055/s-2001-17440

Reference yield:

: 943304-43-6
N-[2-hydroxy-1-(2-octyl-[1,3]dithian-2-yl)-ethyl]-4-methyl-benzenesulfonamide

: 382653-93-2
2-Trimethylsilanyl-ethanesulfonic acid [(R)-1-(2-benzenesulfonyl-ethyl)-decyl]-amide

Guidance literature:: Multi-step reaction with 5 steps

1.1: ethanol / Raney nickel / Heating

2.1: 91 percent / KOH; TsCl / tetrahydrofuran / 20 °C

3.1: Na; naphthalene / tetrahydrofuran / -78 °C

4.1: DMAP; Et₃N / CH₂Cl₂ / 0 °C

5.1: n-BuLi; TMEDA / tetrahydrofuran / -78 °C

5.2: 89 percent / tetrahydrofuran / -78 - 20 °C

With dmap; potassium hydroxide; n-butyllithium; naphthalene; ethanol; N,N,N,N,-tetramethylethylenediamine; sodium; triethylamine; p-toluenesulfonyl chloride; nickel; In tetrahydrofuran; dichloromethane;
DOI:10.1055/s-2001-17440