C₁₇H₂₆N₄O₄SSi

Base Information

• Chemical Name: C₁₇H₂₆N₄O₄SSi
• CAS No.: 1397372-62-1
• Molecular Formula: C₁₇H₂₆N₄O₄SSi
• Molecular Weight: 410.569
• Mol file: 1397372-62-1.mol

Synonyms:C₁₇H₂₆N₄O₄SSi

Chemical Property of C₁₇H₂₆N₄O₄SSi

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₇H₂₆N₄O₄SSi

There total 5 articles about C₁₇H₂₆N₄O₄SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

3-(2-(1-phenyl-1H-tetrazol-5-ylsulfonyl)ethyl)oxiran-2-yl diisopropylcarbamate + t-butyldimethylsiyl triflate (69739-34-0) → C17H26N4O4SSi (1397372-62-1)

Guidance literature:

With 2,6-dimethylpyridine;

DOI:10.1016/j.tetlet.2012.06.142

Reference yield: 67.0%

C17H25N5O3SSi → C17H26N4O4SSi (1397372-62-1)

Guidance literature:

C₁₇H₂₅N₅O₃SSi; With diisobutylaluminium hydride; In toluene; at -78 - -20 ℃; for 4h;

With potassium tartrate sodium salt; In water; for 24h;

DOI:10.1021/acs.joc.8b02033

Reference yield:

(Z)-4-(1-phenyl-1H-tetrazol-5-ylthio)but-1-enyl diisopropylcarbamate (1397372-74-5) → C17H26N4O4SSi (1397372-62-1)

Guidance literature:

Multi-step reaction with 3 steps

1: hexaammonium heptamolybdate tetrahydrate; dihydrogen peroxide / ethanol

2: Oxone; acetone / 20 °C

3: 2,6-dimethylpyridine

With 2,6-dimethylpyridine; Oxone; hexaammonium heptamolybdate tetrahydrate; dihydrogen peroxide; acetone; In ethanol;

DOI:10.1016/j.tetlet.2012.06.142

upstream raw materials:

t-butyldimethylsiyl triflate

(Z)-4-(1-phenyl-1H-tetrazol-5-ylthio)but-1-enyl diisopropylcarbamate

(Z)-4-(1-phenyl-1H-tetrazol-5-ylsulfonyl)but-1-enyl diisopropylcarbamate

1-Phenyl-1H-tetrazole-5-thiol