10-(4-Methoxy-phenyl)-9-[(E)-phenylimino]-1-pyrrol-1-yl-9H-3-thia-4-aza-cyclopenta[b]fluorene-2-carboxylic acid hydrazide

Base Information

Chemical Name:10-(4-Methoxy-phenyl)-9-[(E)-phenylimino]-1-pyrrol-1-yl-9H-3-thia-4-aza-cyclopenta[b]fluorene-2-carboxylic acid hydrazide
CAS No.:204989-29-7
Molecular Formula:C₃₂H₂₃N₅O₂S
Molecular Weight:541.633
Hs Code.:

Synonyms:10-(4-Methoxy-phenyl)-9-[(E)-phenylimino]-1-pyrrol-1-yl-9H-3-thia-4-aza-cyclopenta[b]fluorene-2-carboxylic acid hydrazide

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Chemical Property of 10-(4-Methoxy-phenyl)-9-[(E)-phenylimino]-1-pyrrol-1-yl-9H-3-thia-4-aza-cyclopenta[b]fluorene-2-carboxylic acid hydrazide

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Technology Process of 10-(4-Methoxy-phenyl)-9-[(E)-phenylimino]-1-pyrrol-1-yl-9H-3-thia-4-aza-cyclopenta[b]fluorene-2-carboxylic acid hydrazide

There total 5 articles about 10-(4-Methoxy-phenyl)-9-[(E)-phenylimino]-1-pyrrol-1-yl-9H-3-thia-4-aza-cyclopenta[b]fluorene-2-carboxylic acid hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 204989-28-6
10-(4-Methoxy-phenyl)-9-[(E)-phenylimino]-1-pyrrol-1-yl-9H-3-thia-4-aza-cyclopenta[b]fluorene-2-carboxylic acid ethyl ester

: 204989-29-7
10-(4-Methoxy-phenyl)-9-[(E)-phenylimino]-1-pyrrol-1-yl-9H-3-thia-4-aza-cyclopenta[b]fluorene-2-carboxylic acid hydrazide

Guidance literature:: With hydrazine hydrate; In ethanol; for 1h; Heating;

Reference yield:

: 39145-31-8
2-cyano-3-(4-methoxyphenyl)thioacrylamide

: 204989-29-7
10-(4-Methoxy-phenyl)-9-[(E)-phenylimino]-1-pyrrol-1-yl-9H-3-thia-4-aza-cyclopenta[b]fluorene-2-carboxylic acid hydrazide

Guidance literature:: Multi-step reaction with 4 steps

1: 76 percent / piperidine / ethanol / 6 h / Heating

2: 84 percent / EtONa / ethanol / 1 h / Heating

3: 84 percent / AcOH / 1 h / Heating

4: 78 percent / NH₂NH₂*H₂O / ethanol / 1 h / Heating

With piperidine; sodium ethanolate; hydrazine hydrate; acetic acid; In ethanol;

Reference yield:

: 1-phenyliminoindan-3-one

: 204989-29-7
10-(4-Methoxy-phenyl)-9-[(E)-phenylimino]-1-pyrrol-1-yl-9H-3-thia-4-aza-cyclopenta[b]fluorene-2-carboxylic acid hydrazide

Guidance literature:: Multi-step reaction with 4 steps

1: 76 percent / piperidine / ethanol / 6 h / Heating

2: 84 percent / EtONa / ethanol / 1 h / Heating

3: 84 percent / AcOH / 1 h / Heating

4: 78 percent / NH₂NH₂*H₂O / ethanol / 1 h / Heating

With piperidine; sodium ethanolate; hydrazine hydrate; acetic acid; In ethanol;