1-(4-hydroxyazobenzene-4-oxy)-5-{[(2,3,4-tridodecyloxy)phenylethynyl]phenoxy}-pentane

Base Information

Chemical Name:1-(4-hydroxyazobenzene-4-oxy)-5-{[(2,3,4-tridodecyloxy)phenylethynyl]phenoxy}-pentane
CAS No.:618913-10-3
Molecular Formula:C₆₇H₁₀₀N₂O₆
Molecular Weight:1029.54
Hs Code.:

Synonyms:1-(4-hydroxyazobenzene-4-oxy)-5-{[(2,3,4-tridodecyloxy)phenylethynyl]phenoxy}-pentane

Suppliers and Price of 1-(4-hydroxyazobenzene-4-oxy)-5-{[(2,3,4-tridodecyloxy)phenylethynyl]phenoxy}-pentane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-(4-hydroxyazobenzene-4-oxy)-5-{[(2,3,4-tridodecyloxy)phenylethynyl]phenoxy}-pentane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-(4-hydroxyazobenzene-4-oxy)-5-{[(2,3,4-tridodecyloxy)phenylethynyl]phenoxy}-pentane

There total 12 articles about 1-(4-hydroxyazobenzene-4-oxy)-5-{[(2,3,4-tridodecyloxy)phenylethynyl]phenoxy}-pentane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 618913-09-0
4-[(2,3,4-tridodecyloxy)phenylethynyl]-(5-bromopentyloxy)benzene

: 2050-16-0,51437-66-2
(E)-4,4'-dihydroxyazobenzene

: 618913-10-3
1-(4-hydroxyazobenzene-4-oxy)-5-{[(2,3,4-tridodecyloxy)phenylethynyl]phenoxy}-pentane

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 70 ℃; for 24h;
DOI:10.1080/714965611

Reference yield:

: 103939-79-3
(E)-4-hydroxy-4′-methoxyazobenzene

: 618913-10-3
1-(4-hydroxyazobenzene-4-oxy)-5-{[(2,3,4-tridodecyloxy)phenylethynyl]phenoxy}-pentane

Guidance literature:: Multi-step reaction with 2 steps

1: 40 percent / AlCl₃ / CHCl₃; pyridine / 30 h / Heating

2: 40 percent / K₂CO₃ / dimethylformamide / 24 h / 70 °C

With aluminium trichloride; potassium carbonate; In pyridine; chloroform; N,N-dimethyl-formamide;
DOI:10.1080/714965611

Reference yield:

: 104-94-9
4-methoxy-aniline

: 618913-10-3
1-(4-hydroxyazobenzene-4-oxy)-5-{[(2,3,4-tridodecyloxy)phenylethynyl]phenoxy}-pentane

Guidance literature:: Multi-step reaction with 3 steps

1.1: NaNO₂; conc. H₂SO₄ / H₂O

1.2: NaOH; Na₂CO₃ / H₂O / 0 - 5 °C

2.1: 40 percent / AlCl₃ / CHCl₃; pyridine / 30 h / Heating

3.1: 40 percent / K₂CO₃ / dimethylformamide / 24 h / 70 °C

With aluminium trichloride; sulfuric acid; potassium carbonate; sodium nitrite; In pyridine; chloroform; water; N,N-dimethyl-formamide;
DOI:10.1080/714965611