1,1',3,3'-tetrakis(2,6-dimethylphenyl)-2,2'-bis(1,3,2-diazaphospholidinyl)

Base Information

Chemical Name:1,1',3,3'-tetrakis(2,6-dimethylphenyl)-2,2'-bis(1,3,2-diazaphospholidinyl)
CAS No.:1330191-27-9
Molecular Formula:C₃₆H₄₄N₄P₂
Molecular Weight:594.72
Hs Code.:

Synonyms:1,1',3,3'-tetrakis(2,6-dimethylphenyl)-2,2'-bis(1,3,2-diazaphospholidinyl)

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Chemical Property of 1,1',3,3'-tetrakis(2,6-dimethylphenyl)-2,2'-bis(1,3,2-diazaphospholidinyl)

Chemical Property:

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Technology Process of 1,1',3,3'-tetrakis(2,6-dimethylphenyl)-2,2'-bis(1,3,2-diazaphospholidinyl)

There total 3 articles about 1,1',3,3'-tetrakis(2,6-dimethylphenyl)-2,2'-bis(1,3,2-diazaphospholidinyl) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1330191-23-5
1,3-bis(2,6-dimethylphenyl)-2-(diphenylphosphanyl)-1,3,2-diazaphospholidine

: 1330191-27-9
1,1',3,3'-tetrakis(2,6-dimethylphenyl)-2,2'-bis(1,3,2-diazaphospholidinyl)

: 1101-41-3
Tetraphenyldiphosphin

Guidance literature:: In hexane; at 25 ℃; for 336h; Inert atmosphere;
DOI:10.1002/zaac.201100023

Reference yield:

: 72991-60-7
N¹,N²-bis(2,6-dimethylphenyl)ethane-1,2-diamine

: 1330191-27-9
1,1',3,3'-tetrakis(2,6-dimethylphenyl)-2,2'-bis(1,3,2-diazaphospholidinyl)

Guidance literature:: Multi-step reaction with 2 steps

1: phosphorus trichloride; triethylamine / tetrahydrofuran / 6.25 h / -78 - 20 °C / Inert atmosphere; Schlenk technique; Glovebox

2: magnesium / tetrahydrofuran / 0.24 h / Inert atmosphere; Schlenk technique; Glovebox

With magnesium; triethylamine; phosphorus trichloride; In tetrahydrofuran;
DOI:10.1002/ejic.201201471

Reference yield:

: 674783-84-7
2-chloro-1,3-(2,6-dimethylphenyl)-1,3,2-diazaphospholidine

: 1330191-27-9
1,1',3,3'-tetrakis(2,6-dimethylphenyl)-2,2'-bis(1,3,2-diazaphospholidinyl)

Guidance literature:: With magnesium; In tetrahydrofuran; for 0.24h; Inert atmosphere; Schlenk technique; Glovebox;
DOI:10.1002/ejic.201201471