1,3-bis(2,6-dimethylphenyl)-2-(diphenylphosphanyl)-1,3,2-diazaphospholidine

Base Information

Chemical Name:1,3-bis(2,6-dimethylphenyl)-2-(diphenylphosphanyl)-1,3,2-diazaphospholidine
CAS No.:1330191-23-5
Molecular Formula:C₃₀H₃₂N₂P₂
Molecular Weight:482.545
Hs Code.:

Synonyms:1,3-bis(2,6-dimethylphenyl)-2-(diphenylphosphanyl)-1,3,2-diazaphospholidine

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Chemical Property of 1,3-bis(2,6-dimethylphenyl)-2-(diphenylphosphanyl)-1,3,2-diazaphospholidine

Chemical Property:

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Technology Process of 1,3-bis(2,6-dimethylphenyl)-2-(diphenylphosphanyl)-1,3,2-diazaphospholidine

There total 3 articles about 1,3-bis(2,6-dimethylphenyl)-2-(diphenylphosphanyl)-1,3,2-diazaphospholidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 674783-84-7
2-chloro-1,3-(2,6-dimethylphenyl)-1,3,2-diazaphospholidine

: 829-85-6
diphenylphosphane

: 1330191-23-5
1,3-bis(2,6-dimethylphenyl)-2-(diphenylphosphanyl)-1,3,2-diazaphospholidine

Guidance literature:: diphenylphosphane; With n-butyllithium; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 0.783333h;

2-chloro-1,3-(2,6-dimethylphenyl)-1,3,2-diazaphospholidine; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 0.833333h;
DOI:10.1002/zaac.201100023

Reference yield:

: 72991-60-7
N¹,N²-bis(2,6-dimethylphenyl)ethane-1,2-diamine

: 1330191-23-5
1,3-bis(2,6-dimethylphenyl)-2-(diphenylphosphanyl)-1,3,2-diazaphospholidine

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine; phosphorus trichloride / tetrahydrofuran / -78 - 25 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.78 h / -78 - 20 °C

2.2: 0.83 h / -78 - 20 °C

With n-butyllithium; triethylamine; phosphorus trichloride; In tetrahydrofuran; hexane;
DOI:10.1002/zaac.201100023

Reference yield:

: 49673-43-0
N¹,N²-bis(2,6-dimethylphenyl)ethane-1,2-diimine

: 1330191-23-5
1,3-bis(2,6-dimethylphenyl)-2-(diphenylphosphanyl)-1,3,2-diazaphospholidine

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium aluminium tetrahydride / diethyl ether / -78 °C

2.1: triethylamine; phosphorus trichloride / tetrahydrofuran / -78 - 25 °C

3.1: n-butyllithium / tetrahydrofuran; hexane / 0.78 h / -78 - 20 °C

3.2: 0.83 h / -78 - 20 °C

With lithium aluminium tetrahydride; n-butyllithium; triethylamine; phosphorus trichloride; In tetrahydrofuran; diethyl ether; hexane;
DOI:10.1002/zaac.201100023