Technology Process of meso-5-mono-o-propynamidophenyl-10,15,20-triphenylporphyriniron(III) chloride
There total 1 articles about meso-5-mono-o-propynamidophenyl-10,15,20-triphenylporphyriniron(III) chloride which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
oxygen;
In
tetrahydrofuran; methanol; benzene;
FeBr2 added to free-base porphyrin in CH3OH-THF, reflux for 45 min, cooled to room temp., air bubbled for 1 h, benzene added, hydrolyzed by eashing with 8% HCl; solvents distilled, TLC (Al2O3, hexane/ethyl acetate 2:1 v/v);
DOI:10.1021/jp057416p