N-benzyloxycarbonyl-α-(p-nitrobenzyl)-(Z)-α,β-dehydroglutamic-γ-O-(p-nitrobenzyl)hydroxamic acid

Base Information

Chemical Name:N-benzyloxycarbonyl-α-(p-nitrobenzyl)-(Z)-α,β-dehydroglutamic-γ-O-(p-nitrobenzyl)hydroxamic acid
CAS No.:105933-68-4
Molecular Formula:C₂₇H₂₄N₄O₁₀
Molecular Weight:564.508
Hs Code.:

Synonyms:N-benzyloxycarbonyl-α-(p-nitrobenzyl)-(Z)-α,β-dehydroglutamic-γ-O-(p-nitrobenzyl)hydroxamic acid

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Chemical Property of N-benzyloxycarbonyl-α-(p-nitrobenzyl)-(Z)-α,β-dehydroglutamic-γ-O-(p-nitrobenzyl)hydroxamic acid

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Technology Process of N-benzyloxycarbonyl-α-(p-nitrobenzyl)-(Z)-α,β-dehydroglutamic-γ-O-(p-nitrobenzyl)hydroxamic acid

There total 7 articles about N-benzyloxycarbonyl-α-(p-nitrobenzyl)-(Z)-α,β-dehydroglutamic-γ-O-(p-nitrobenzyl)hydroxamic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 104754-51-0
N-benzyloxycarbonyl-2-aminotetrahydro-5-oxo-2-furancarboxylic acid

: 105933-68-4
N-benzyloxycarbonyl-α-(p-nitrobenzyl)-(Z)-α,β-dehydroglutamic-γ-O-(p-nitrobenzyl)hydroxamic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent

2: DBU / tetrahydrofuran / 0 °C

3: 60 percent

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran;
DOI:10.1021/ja00394a039

Reference yield:

: 104754-60-1
p-nitrobenzyl-N-benzyloxycarbonyl-2-aminotetrahydro-5-oxo-2-furancarboxylate

: 105933-68-4
N-benzyloxycarbonyl-α-(p-nitrobenzyl)-(Z)-α,β-dehydroglutamic-γ-O-(p-nitrobenzyl)hydroxamic acid

Guidance literature:: Multi-step reaction with 2 steps

1: DBU / tetrahydrofuran / 0 °C

2: 60 percent

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran;
DOI:10.1021/ja00394a039

Reference yield:

: 100-11-8
1-bromomethyl-4-nitro-benzene

: 105933-68-4
N-benzyloxycarbonyl-α-(p-nitrobenzyl)-(Z)-α,β-dehydroglutamic-γ-O-(p-nitrobenzyl)hydroxamic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent

2: DBU / tetrahydrofuran / 0 °C

3: 60 percent

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran;
DOI:10.1021/ja00394a039