1-(5-(3-hydroxy-4-methoxyphenyl)-3-(3,4,5-trimethoxyphenyl)-1H-pyrazol-1-yl)ethanone

Base Information

• Chemical Name: 1-(5-(3-hydroxy-4-methoxyphenyl)-3-(3,4,5-trimethoxyphenyl)-1H-pyrazol-1-yl)ethanone
• CAS No.: 1392307-41-3
• Molecular Formula: C₂₁H₂₂N₂O₆
• Molecular Weight: 398.415

Synonyms:1-(5-(3-hydroxy-4-methoxyphenyl)-3-(3,4,5-trimethoxyphenyl)-1H-pyrazol-1-yl)ethanone

Chemical Property of 1-(5-(3-hydroxy-4-methoxyphenyl)-3-(3,4,5-trimethoxyphenyl)-1H-pyrazol-1-yl)ethanone

Chemical Property:

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Technology Process of 1-(5-(3-hydroxy-4-methoxyphenyl)-3-(3,4,5-trimethoxyphenyl)-1H-pyrazol-1-yl)ethanone

There total 4 articles about 1-(5-(3-hydroxy-4-methoxyphenyl)-3-(3,4,5-trimethoxyphenyl)-1H-pyrazol-1-yl)ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

isovanillin (621-59-0) → 1-(5-(3-hydroxy-4-methoxyphenyl)-3-(3,4,5-trimethoxyphenyl)-1H-pyrazol-1-yl)ethanone (1392307-41-3)

Guidance literature:

Multi-step reaction with 3 steps

1: water; potassium hydroxide / ethanol

2: acetic acid; hydrazine hydrate / Reflux

3: acetic acid / 50 °C

With water; hydrazine hydrate; acetic acid; potassium hydroxide; In ethanol;

Reference yield:

methyl (3,4,5-trimethoxyphenyl) ketone (1136-86-3) → 1-(5-(3-hydroxy-4-methoxyphenyl)-3-(3,4,5-trimethoxyphenyl)-1H-pyrazol-1-yl)ethanone (1392307-41-3)

Guidance literature:

Multi-step reaction with 3 steps

1: water; potassium hydroxide / ethanol

2: acetic acid; hydrazine hydrate / Reflux

3: acetic acid / 50 °C

With water; hydrazine hydrate; acetic acid; potassium hydroxide; In ethanol;

Reference yield:

1-(5-(3-hydroxy-4-methoxyphenyl)-3-(3,4,5-trimethoxyphenyl)-4,5-dihydro-1H-pyrazol-1-yl)ethanone → 1-(5-(3-hydroxy-4-methoxyphenyl)-3-(3,4,5-trimethoxyphenyl)-1H-pyrazol-1-yl)ethanone (1392307-41-3)

Guidance literature:

With acetic acid; at 50 ℃;

upstream raw materials:

isovanillin

methyl (3,4,5-trimethoxyphenyl) ketone

(E)-3-(3-hydroxy-4-methoxyphenyl)-1-(3,4,5-trimethoxyphenyl)prop-2-en-1-one

Downstream raw materials:

1-[5-(3-{[3-(4-{3-[4-(1,3-benzothiazol-2-yl)-2-methoxyphenoxy]propyl}piperazino)propyl]oxy}-4-methoxyphenyl)-3-(3,4,5-trimethoxyphenyl)-1H-1-pyrazolyl]-1-ethanone

1-[5-(3-{3-[4-(1,3-benzothiazol-2-yl)-2-methoxyphenoxy]propoxy}-4-methoxyphenyl)-3-(3,4,5-trimethoxyphenyl)-1H-1-pyrazolyl]-1-ethanone

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