4-<carbonyl>-2-(1,1-dimethylethyl)phenyl octadecylcarbamate

Base Information

Chemical Name:4-<carbonyl>-2-(1,1-dimethylethyl)phenyl octadecylcarbamate
CAS No.:147219-66-7
Molecular Formula:C₃₈H₅₉N₃O₄
Molecular Weight:621.904
Hs Code.:

4-<<acetyl(2-pyridinylmethyl)amino>carbonyl>-2-(1,1-dimethylethyl)phenyl octadecylcarbamate

Synonyms:4-<carbonyl>-2-(1,1-dimethylethyl)phenyl octadecylcarbamate

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Chemical Property of 4-<carbonyl>-2-(1,1-dimethylethyl)phenyl octadecylcarbamate

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Technology Process of 4-<carbonyl>-2-(1,1-dimethylethyl)phenyl octadecylcarbamate

There total 7 articles about 4-<carbonyl>-2-(1,1-dimethylethyl)phenyl octadecylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 112-96-9
octadecyl isocyanate

: 147236-25-7
N-acetyl-3-(1,1-dimethylethyl)-4-hydroxy-N-(2-pyridinylmethyl)benzamide

: 147219-66-7
4-<carbonyl>-2-(1,1-dimethylethyl)phenyl octadecylcarbamate

Guidance literature:: With triethylamine; In tetrahydrofuran; for 22h; Ambient temperature;
DOI:10.1021/jm00057a008

Reference yield:

: 3731-51-9
2-(Aminomethyl)pyridine

: 147219-66-7
4-<carbonyl>-2-(1,1-dimethylethyl)phenyl octadecylcarbamate

Guidance literature:: Multi-step reaction with 4 steps

1: 4-(dimethylamino)pyridine, pyridine / 92 h / Ambient temperature

2: 1.) sodium hydride, HMPA / 1.) THF, 0 deg C, 15 min, 2.) THF, RT, 3.5 h

3: 81 percent / tetrabutylammonium fluoride / tetrahydrofuran / 1.) 0 deg C, 15 min, 2.) RT, 3 h

4: 88 percent / triethylamine / tetrahydrofuran / 22 h / Ambient temperature

With pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; dmap; tetrabutyl ammonium fluoride; sodium hydride; triethylamine; In tetrahydrofuran;
DOI:10.1021/jm00057a008

Reference yield:

: 58481-18-8
N-(pyridin-2-ylmethyl)acetamide

: 147219-66-7
4-<carbonyl>-2-(1,1-dimethylethyl)phenyl octadecylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) sodium hydride, HMPA / 1.) THF, 0 deg C, 15 min, 2.) THF, RT, 3.5 h

2: 81 percent / tetrabutylammonium fluoride / tetrahydrofuran / 1.) 0 deg C, 15 min, 2.) RT, 3 h

3: 88 percent / triethylamine / tetrahydrofuran / 22 h / Ambient temperature

With N,N,N,N,N,N-hexamethylphosphoric triamide; tetrabutyl ammonium fluoride; sodium hydride; triethylamine; In tetrahydrofuran;
DOI:10.1021/jm00057a008