3-(benzyloxymethyl)-2-methyl-2-(t-butyldimethylsilyl)propanal

Base Information

Chemical Name:3-(benzyloxymethyl)-2-methyl-2-(t-butyldimethylsilyl)propanal
CAS No.:1611465-64-5
Molecular Formula:C₁₇H₂₈O₃Si
Molecular Weight:308.493
Hs Code.:

Synonyms:3-(benzyloxymethyl)-2-methyl-2-(t-butyldimethylsilyl)propanal

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Chemical Property of 3-(benzyloxymethyl)-2-methyl-2-(t-butyldimethylsilyl)propanal

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Technology Process of 3-(benzyloxymethyl)-2-methyl-2-(t-butyldimethylsilyl)propanal

There total 6 articles about 3-(benzyloxymethyl)-2-methyl-2-(t-butyldimethylsilyl)propanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 88-67-5
2-Iodobenzoic acid

: 1611466-28-4
3-(benzyloxy)methyl-2-methyl-2-(t-butyldimethylsilyl)propanol

: 1611465-64-5
3-(benzyloxymethyl)-2-methyl-2-(t-butyldimethylsilyl)propanal

Guidance literature:: In ethyl acetate; at 0 - 80 ℃; for 8h;
DOI:10.1002/chem.201304776

Reference yield:

: 53159-33-4
5-hydroxy-5-methyl-2-phenyl-1,3-dioxane

: 1611465-64-5
3-(benzyloxymethyl)-2-methyl-2-(t-butyldimethylsilyl)propanal

Guidance literature:: Multi-step reaction with 3 steps

1: dmap / 20 °C

2: sodium cyanoborohydride; titanium tetrachloride / acetonitrile / 2 h / -35 °C

3: ethyl acetate / 8 h / 0 - 80 °C

With dmap; titanium tetrachloride; sodium cyanoborohydride; In ethyl acetate; acetonitrile;
DOI:10.1002/chem.201304776

Reference yield:

: 51430-74-1
5-amino-5-hydroxymethyl-2-phenyl-1,3-dioxane

: 1611465-64-5
3-(benzyloxymethyl)-2-methyl-2-(t-butyldimethylsilyl)propanal

Guidance literature:: Multi-step reaction with 5 steps

1: potassium dihydrogenphosphate; sodium periodate / methanol; water / 0 - 20 °C

2: ethylene dibromide; magnesium / diethyl ether / 0.5 h / 20 °C

3: dmap / 20 °C

4: sodium cyanoborohydride; titanium tetrachloride / acetonitrile / 2 h / -35 °C

5: ethyl acetate / 8 h / 0 - 80 °C

With dmap; sodium periodate; potassium dihydrogenphosphate; titanium tetrachloride; sodium cyanoborohydride; magnesium; ethylene dibromide; In methanol; diethyl ether; water; ethyl acetate; acetonitrile;
DOI:10.1002/chem.201304776