(S)-2-methylsulfonyloxy-1-phenyl-1-propanone 2,2-dimethyl-trimethylene acetal

Base Information

Chemical Name:(S)-2-methylsulfonyloxy-1-phenyl-1-propanone 2,2-dimethyl-trimethylene acetal
CAS No.:103624-14-2
Molecular Formula:C₁₅H₂₂O₅S
Molecular Weight:314.403
Hs Code.:

Synonyms:(S)-2-methylsulfonyloxy-1-phenyl-1-propanone 2,2-dimethyl-trimethylene acetal

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Chemical Property of (S)-2-methylsulfonyloxy-1-phenyl-1-propanone 2,2-dimethyl-trimethylene acetal

Chemical Property:

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Technology Process of (S)-2-methylsulfonyloxy-1-phenyl-1-propanone 2,2-dimethyl-trimethylene acetal

There total 5 articles about (S)-2-methylsulfonyloxy-1-phenyl-1-propanone 2,2-dimethyl-trimethylene acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 124-63-0
methanesulfonyl chloride

: 111197-86-5
(S)-2-hydroxy-1-phenyl-1-propanone 2,2-dimethyl-trimethylene acetal

: 103624-14-2
(S)-2-methylsulfonyloxy-1-phenyl-1-propanone 2,2-dimethyl-trimethylene acetal

Guidance literature:: With pyridine; for 12h; Ambient temperature;
DOI:10.1246/bcsj.60.1027

Reference yield:

: 5650-40-8,65646-06-2,91840-95-8,65646-07-3
(S)-2-hydroxypropiophenone

: 103624-14-2
(S)-2-methylsulfonyloxy-1-phenyl-1-propanone 2,2-dimethyl-trimethylene acetal

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / trimethylchlorosilane / methanol / 2 h / ice bath

2: 98 percent / pyridine / 12 h / Ambient temperature

With pyridine; chloro-trimethyl-silane; In methanol;
DOI:10.1246/bcsj.60.1027

Reference yield:

: (S)-2-(1-ethoxyethoxy)-1-phenyl-1-propanone

: 103624-14-2
(S)-2-methylsulfonyloxy-1-phenyl-1-propanone 2,2-dimethyl-trimethylene acetal

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / PPTS / ethanol / 6 h

2: 89 percent / trimethylchlorosilane / methanol / 2 h / ice bath

3: 98 percent / pyridine / 12 h / Ambient temperature

With pyridine; chloro-trimethyl-silane; pyridinium p-toluenesulfonate; In methanol; ethanol;
DOI:10.1246/bcsj.60.1027