methyl 6-[(R/S)-1-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)ethyl]phenazine-1-carboxylic ester

Base Information

Chemical Name:methyl 6-[(R/S)-1-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)ethyl]phenazine-1-carboxylic ester
CAS No.:639067-01-9
Molecular Formula:C₅₀H₄₀N₂O₁₂
Molecular Weight:860.874
Hs Code.:

Synonyms:methyl 6-[(R/S)-1-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)ethyl]phenazine-1-carboxylic ester

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Chemical Property of methyl 6-[(R/S)-1-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)ethyl]phenazine-1-carboxylic ester

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Technology Process of methyl 6-[(R/S)-1-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)ethyl]phenazine-1-carboxylic ester

There total 3 articles about methyl 6-[(R/S)-1-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)ethyl]phenazine-1-carboxylic ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 73634-72-7
Saphenic acid methyl ester

: 2,4-dinitro-6-(methoxycarbonyl)phenyl 2,3,4,6-tetra-O-benzoyl-α/β-D-glucopyranoside

: 639067-01-9
methyl 6-[(R/S)-1-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)ethyl]phenazine-1-carboxylic ester

Guidance literature:: With 4 A molecular sieve; lithium perchlorate; In nitromethane; at 20 - 50 ℃; for 19.5h;
DOI:10.1039/b306789k

Reference yield:

: 627466-64-2
2,3,4,6-tetra-O-benzoyl-D-glucopyranose

: 639067-01-9
methyl 6-[(R/S)-1-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)ethyl]phenazine-1-carboxylic ester

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / Li₂CO₃; DMAP / CH₂Cl₂ / 0.17 h

2: 65 percent / LiClO₄; 4 Angstroem molecular sieves / nitromethane / 19.5 h / 20 - 50 °C

With dmap; 4 A molecular sieve; lithium perchlorate; lithium carbonate; In nitromethane; dichloromethane;
DOI:10.1039/b306789k

Reference yield:

: 123806-73-5
6-(1-hydroxyethyl)-phenazine-1-carboxylic acid

: 639067-01-9
methyl 6-[(R/S)-1-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)ethyl]phenazine-1-carboxylic ester

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl chloride

2: 65 percent / LiClO₄; 4 Angstroem molecular sieves / nitromethane / 19.5 h / 20 - 50 °C

With oxalyl dichloride; 4 A molecular sieve; lithium perchlorate; In nitromethane;
DOI:10.1039/b306789k