Technology Process of C33H35NO6
There total 10 articles about C33H35NO6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / Reflux
2: ethanol / 14 h / Reflux
With
lithium aluminium tetrahydride;
In
tetrahydrofuran; ethanol;
DOI:10.1016/j.bmc.2012.12.016
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium hydroxide; water; copper; copper(II) oxide / 1 h / 140 °C / Inert atmosphere; Microwave irradiation
2.1: phenylboronic acid / toluene / 1 h / Reflux; Dean-Stark
2.2: 46 h / 100 °C / Molecular sieve; Sealed tube
2.3: 2 h / Reflux
3.1: potassium carbonate / acetone / 4 h / Reflux
4.1: ethanol / 14 h / Reflux
With
water; copper; potassium carbonate; copper(II) oxide; potassium hydroxide; phenylboronic acid;
In
ethanol; acetone; toluene;
DOI:10.1016/j.bmc.2012.12.016
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: phenylboronic acid / toluene / 1 h / Reflux; Dean-Stark
1.2: 46 h / 100 °C / Molecular sieve; Sealed tube
1.3: 2 h / Reflux
2.1: potassium carbonate / acetone / 4 h / Reflux
3.1: ethanol / 14 h / Reflux
With
potassium carbonate; phenylboronic acid;
In
ethanol; acetone; toluene;
DOI:10.1016/j.bmc.2012.12.016