(Benzyloxycarbonylmethyl-tert-butoxycarbonylmethyl-amino)-acetic acid tert-butyl ester

Base Information

• Chemical Name: (Benzyloxycarbonylmethyl-tert-butoxycarbonylmethyl-amino)-acetic acid tert-butyl ester
• CAS No.: 171557-57-6
• Molecular Formula: C₂₁H₃₁NO₆
• Molecular Weight: 393.48

Synonyms:(Benzyloxycarbonylmethyl-tert-butoxycarbonylmethyl-amino)-acetic acid tert-butyl ester

Chemical Property of (Benzyloxycarbonylmethyl-tert-butoxycarbonylmethyl-amino)-acetic acid tert-butyl ester

Chemical Property:

Purity/Quality:

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SDS file from LookChem

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Technology Process of (Benzyloxycarbonylmethyl-tert-butoxycarbonylmethyl-amino)-acetic acid tert-butyl ester

There total 2 articles about (Benzyloxycarbonylmethyl-tert-butoxycarbonylmethyl-amino)-acetic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

bromoacetic acid tert-butyl ester (5292-43-3) + benzyl 2-aminoacetate hydrochloride (2462-31-9) → (Benzyloxycarbonylmethyl-tert-butoxycarbonylmethyl-amino)-acetic acid tert-butyl ester (171557-57-6)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 60 ℃;

DOI:10.1016/j.bmcl.2014.04.096

Reference yield:

glycine benzyl ester p-toluenesulfonic acid salt (1738-76-7) + t-butyl iodoacetate (49827-15-8) → (Benzyloxycarbonylmethyl-tert-butoxycarbonylmethyl-amino)-acetic acid tert-butyl ester (171557-57-6)

Guidance literature:

With pH 7.0 phosphate buffer; In dimethyl sulfoxide; for 48h;

DOI:10.1021/jo00126a059

Reference yield: 97.0%

(Benzyloxycarbonylmethyl-tert-butoxycarbonylmethyl-amino)-acetic acid tert-butyl ester (171557-57-6) → 2-[bis(2-tert-butoxy-2-oxoethyl)amino]acetic acid (171557-31-6)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In methanol; at 20 ℃; for 2h;

DOI:10.1016/j.bmcl.2014.04.096

upstream raw materials:

glycine benzyl ester p-toluenesulfonic acid salt

t-butyl iodoacetate

bromoacetic acid tert-butyl ester

benzyl 2-aminoacetate hydrochloride

Downstream raw materials:

2-[bis(2-tert-butoxy-2-oxoethyl)amino]acetic acid

C₃₄H₅₅N₅O₁₀

C₁₈H₂₃N₅O₁₀

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