(E)-di-tert-butyl (4-(1-phenyl-1H-tetrazol-5-ylthio)but-2-enyl)iminodicarbonate

Base Information

Chemical Name:(E)-di-tert-butyl (4-(1-phenyl-1H-tetrazol-5-ylthio)but-2-enyl)iminodicarbonate
CAS No.:1083003-61-5
Molecular Formula:C₂₁H₂₉N₅O₄S
Molecular Weight:447.558
Hs Code.:

Synonyms:(E)-di-tert-butyl (4-(1-phenyl-1H-tetrazol-5-ylthio)but-2-enyl)iminodicarbonate

Suppliers and Price of (E)-di-tert-butyl (4-(1-phenyl-1H-tetrazol-5-ylthio)but-2-enyl)iminodicarbonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-di-tert-butyl (4-(1-phenyl-1H-tetrazol-5-ylthio)but-2-enyl)iminodicarbonate

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Technology Process of (E)-di-tert-butyl (4-(1-phenyl-1H-tetrazol-5-ylthio)but-2-enyl)iminodicarbonate

There total 1 articles about (E)-di-tert-butyl (4-(1-phenyl-1H-tetrazol-5-ylthio)but-2-enyl)iminodicarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 86-93-1
1-Phenyl-1H-tetrazole-5-thiol

: 121030-31-7
C₁₄H₂₄ClNO₄

: 1083003-61-5
(E)-di-tert-butyl (4-(1-phenyl-1H-tetrazol-5-ylthio)but-2-enyl)iminodicarbonate

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 20 ℃; for 7h;
DOI:10.1055/s-2008-1078011

Reference yield: 95.0%

: 1083003-61-5
(E)-di-tert-butyl (4-(1-phenyl-1H-tetrazol-5-ylthio)but-2-enyl)iminodicarbonate

: 1083003-47-7
C₁₆H₂₁N₅O₂S

Guidance literature:: With methoxybenzene; trifluoroacetic acid; In tetrahydrofuran; for 0.5h;
DOI:10.1055/s-2008-1078011

Reference yield: 83.0%

: 1083003-61-5
(E)-di-tert-butyl (4-(1-phenyl-1H-tetrazol-5-ylthio)but-2-enyl)iminodicarbonate

: 1352406-05-3
(E)-4-(1-phenyl-1H-tetrazol-5-ylthio) but-2-en-1-amine

Guidance literature:: (E)-di-tert-butyl (4-(1-phenyl-1H-tetrazol-5-ylthio)but-2-enyl)iminodicarbonate; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 12h;

With sodium hydrogencarbonate; In dichloromethane; water; at 0 ℃;
DOI:10.1016/j.tet.2011.09.037