(9H-fluoren-9-yl)methyl (E)-4-(1-phenyl-1H-tetrazol-5-ylthio) but-2-enylcarbamate

Base Information

Chemical Name:(9H-fluoren-9-yl)methyl (E)-4-(1-phenyl-1H-tetrazol-5-ylthio) but-2-enylcarbamate
CAS No.:1352406-07-5
Molecular Formula:C₂₆H₂₃N₅O₂S
Molecular Weight:469.567
Hs Code.:

Synonyms:(9H-fluoren-9-yl)methyl (E)-4-(1-phenyl-1H-tetrazol-5-ylthio) but-2-enylcarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (9H-fluoren-9-yl)methyl (E)-4-(1-phenyl-1H-tetrazol-5-ylthio) but-2-enylcarbamate

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Technology Process of (9H-fluoren-9-yl)methyl (E)-4-(1-phenyl-1H-tetrazol-5-ylthio) but-2-enylcarbamate

There total 2 articles about (9H-fluoren-9-yl)methyl (E)-4-(1-phenyl-1H-tetrazol-5-ylthio) but-2-enylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1352406-05-3
(E)-4-(1-phenyl-1H-tetrazol-5-ylthio) but-2-en-1-amine

: 28920-43-6
(fluorenylmethoxy)carbonyl chloride

: 1352406-07-5
(9H-fluoren-9-yl)methyl (E)-4-(1-phenyl-1H-tetrazol-5-ylthio) but-2-enylcarbamate

Guidance literature:: With sodium hydrogencarbonate; In tetrahydrofuran; water; at 20 ℃; for 1h;
DOI:10.1016/j.tet.2011.09.037

Reference yield:

: 1083003-61-5
(E)-di-tert-butyl (4-(1-phenyl-1H-tetrazol-5-ylthio)but-2-enyl)iminodicarbonate

: 1352406-07-5
(9H-fluoren-9-yl)methyl (E)-4-(1-phenyl-1H-tetrazol-5-ylthio) but-2-enylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: trifluoroacetic acid / dichloromethane / 12 h / 20 °C

1.2: 0 °C

2.1: sodium hydrogencarbonate / tetrahydrofuran; water / 1 h / 20 °C

With sodium hydrogencarbonate; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; water;
DOI:10.1016/j.tet.2011.09.037

Reference yield: 54.0%

: 1352406-07-5
(9H-fluoren-9-yl)methyl (E)-4-(1-phenyl-1H-tetrazol-5-ylthio) but-2-enylcarbamate

: 1352405-57-2
(9H-fluoren-9-yl)methyl (E)-4-(1-phenyl-1H-tetrazol-5-ylsulfonyl)but-2-enylcarbamate

Guidance literature:: With hexaammonium heptamolybdate tetrahydrate; dihydrogen peroxide; In ethanol; water; at 20 ℃; for 7h;
DOI:10.1016/j.tet.2011.09.037