(4-ethoxycarbonylamino-1,4-bis-methoxy-methoxymethyl-cyclohexyl)-carbamic acid ethyl ester

Base Information

Chemical Name:(4-ethoxycarbonylamino-1,4-bis-methoxy-methoxymethyl-cyclohexyl)-carbamic acid ethyl ester
CAS No.:896473-10-2
Molecular Formula:C₁₈H₃₄N₂O₈
Molecular Weight:406.477
Hs Code.:

Synonyms:(4-ethoxycarbonylamino-1,4-bis-methoxy-methoxymethyl-cyclohexyl)-carbamic acid ethyl ester

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Chemical Property of (4-ethoxycarbonylamino-1,4-bis-methoxy-methoxymethyl-cyclohexyl)-carbamic acid ethyl ester

Chemical Property:

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Technology Process of (4-ethoxycarbonylamino-1,4-bis-methoxy-methoxymethyl-cyclohexyl)-carbamic acid ethyl ester

There total 5 articles about (4-ethoxycarbonylamino-1,4-bis-methoxy-methoxymethyl-cyclohexyl)-carbamic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1,4-bis-methoxymethoxymethyl-2,3-diaza-bicyclo[2.2.2]octane-2,3-dicarboxylic acid diethyl ester

: 896473-10-2
(4-ethoxycarbonylamino-1,4-bis-methoxy-methoxymethyl-cyclohexyl)-carbamic acid ethyl ester

Guidance literature:: With ammonia; sodium; In tetrahydrofuran; at -70 ℃; for 1h;
DOI:10.1016/j.tet.2006.03.038

Reference yield:

: 896473-07-7
(4-hydroxymethyl-cyclohexa-1,3-dienyl)-methanol

: 896473-10-2
(4-ethoxycarbonylamino-1,4-bis-methoxy-methoxymethyl-cyclohexyl)-carbamic acid ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 36 percent / CH₂Cl₂ / 24 h / 20 °C

2: 95 percent / DIPEA / CH₂Cl₂ / 24 h / 20 °C

3: H₂ / Pd/C / CH₂Cl₂ / 24 h / 20 °C / 517.15 Torr

4: 0.52 g / Na; NH₃ / tetrahydrofuran / 1 h / -70 °C

With ammonia; hydrogen; sodium; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; 1: Diels-Alder reaction;
DOI:10.1016/j.tet.2006.03.038

Reference yield:

: 1,4-bis-hydroxymethyl-2,3-diaza-bicyclo[2.2.2]oct-5-ene-2,3-dicarboxylic acid diethyl ester

: 896473-10-2
(4-ethoxycarbonylamino-1,4-bis-methoxy-methoxymethyl-cyclohexyl)-carbamic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / DIPEA / CH₂Cl₂ / 24 h / 20 °C

2: H₂ / Pd/C / CH₂Cl₂ / 24 h / 20 °C / 517.15 Torr

3: 0.52 g / Na; NH₃ / tetrahydrofuran / 1 h / -70 °C

With ammonia; hydrogen; sodium; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tet.2006.03.038