tert-butyl 5-(acetoxy(3-iodophenyl)amino)-2-(ethoxycarbonothioylthio)-5-oxopentylcarbamate

Base Information

Chemical Name:tert-butyl 5-(acetoxy(3-iodophenyl)amino)-2-(ethoxycarbonothioylthio)-5-oxopentylcarbamate
CAS No.:1403889-69-9
Molecular Formula:C₂₁H₂₉IN₂O₆S₂
Molecular Weight:596.508
Hs Code.:

Synonyms:tert-butyl 5-(acetoxy(3-iodophenyl)amino)-2-(ethoxycarbonothioylthio)-5-oxopentylcarbamate

Suppliers and Price of tert-butyl 5-(acetoxy(3-iodophenyl)amino)-2-(ethoxycarbonothioylthio)-5-oxopentylcarbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of tert-butyl 5-(acetoxy(3-iodophenyl)amino)-2-(ethoxycarbonothioylthio)-5-oxopentylcarbamate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of tert-butyl 5-(acetoxy(3-iodophenyl)amino)-2-(ethoxycarbonothioylthio)-5-oxopentylcarbamate

There total 5 articles about tert-butyl 5-(acetoxy(3-iodophenyl)amino)-2-(ethoxycarbonothioylthio)-5-oxopentylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1403889-61-1
S-2-(acetoxy(3-iodophenyl)amino)-2-oxoethyl O-ethyl carbonodithioate

: 78888-18-3
N-tert-butoxycarbonylprop-2-en-1-amine

: 1403889-69-9
tert-butyl 5-(acetoxy(3-iodophenyl)amino)-2-(ethoxycarbonothioylthio)-5-oxopentylcarbamate

Guidance literature:: With dilauryl peroxide; In ethyl acetate; for 5h; Reflux; Inert atmosphere;
DOI:10.1021/ol3026044

Reference yield:

: 645-00-1
m-iodonitrobenzene

: 1403889-69-9
tert-butyl 5-(acetoxy(3-iodophenyl)amino)-2-(ethoxycarbonothioylthio)-5-oxopentylcarbamate

Guidance literature:: Multi-step reaction with 5 steps

1: ammonium chloride; zinc / ethanol; water / 4 h / 10 °C / Cooling with ice; Inert atmosphere

2: sodium hydrogencarbonate / diethyl ether; water / -5 °C / Cooling with ice; Inert atmosphere

3: acetic anhydride / 20 °C / Inert atmosphere

4: acetone / 6 h / Inert atmosphere

5: dilauryl peroxide / ethyl acetate / 5 h / Reflux; Inert atmosphere

With dilauryl peroxide; acetic anhydride; sodium hydrogencarbonate; ammonium chloride; zinc; In diethyl ether; ethanol; water; ethyl acetate; acetone;
DOI:10.1021/ol3026044

Reference yield:

: 1403889-50-8
N-(3-iodophenyl)-2-chloro-N-hydroxyacetamide

: 1403889-69-9
tert-butyl 5-(acetoxy(3-iodophenyl)amino)-2-(ethoxycarbonothioylthio)-5-oxopentylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: acetic anhydride / 20 °C / Inert atmosphere

2: acetone / 6 h / Inert atmosphere

3: dilauryl peroxide / ethyl acetate / 5 h / Reflux; Inert atmosphere

With dilauryl peroxide; acetic anhydride; In ethyl acetate; acetone;
DOI:10.1021/ol3026044