[4,6-dihydroxy-2-methoxymethoxy-3-(3-methyl-but-2-enyl)-phenyl]-(2,4-dihydroxy-5-methoxy-phenyl)-methanone

Base Information

Chemical Name:[4,6-dihydroxy-2-methoxymethoxy-3-(3-methyl-but-2-enyl)-phenyl]-(2,4-dihydroxy-5-methoxy-phenyl)-methanone
CAS No.:622390-73-2
Molecular Formula:C₂₁H₂₄O₈
Molecular Weight:404.417
Hs Code.:

Synonyms:[4,6-dihydroxy-2-methoxymethoxy-3-(3-methyl-but-2-enyl)-phenyl]-(2,4-dihydroxy-5-methoxy-phenyl)-methanone

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Chemical Property of [4,6-dihydroxy-2-methoxymethoxy-3-(3-methyl-but-2-enyl)-phenyl]-(2,4-dihydroxy-5-methoxy-phenyl)-methanone

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Technology Process of [4,6-dihydroxy-2-methoxymethoxy-3-(3-methyl-but-2-enyl)-phenyl]-(2,4-dihydroxy-5-methoxy-phenyl)-methanone

There total 8 articles about [4,6-dihydroxy-2-methoxymethoxy-3-(3-methyl-but-2-enyl)-phenyl]-(2,4-dihydroxy-5-methoxy-phenyl)-methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 622390-85-6
[4,6-bis-benzyloxy-2-methoxymethoxy-3-(3-methyl-but-2-enyl)-phenyl]-(2,4-bis-benzyloxy-5-methoxy-phenyl)-methanone

: 622390-73-2
[4,6-dihydroxy-2-methoxymethoxy-3-(3-methyl-but-2-enyl)-phenyl]-(2,4-dihydroxy-5-methoxy-phenyl)-methanone

Guidance literature:: With palladium on activated charcoal; ammonium formate; In acetone;
DOI:10.1016/S0960-894X(03)00719-4

Reference yield:

: 6195-80-8
2,4-bis(benzyloxy)phenol

: 622390-73-2
[4,6-dihydroxy-2-methoxymethoxy-3-(3-methyl-but-2-enyl)-phenyl]-(2,4-dihydroxy-5-methoxy-phenyl)-methanone

Guidance literature:: Multi-step reaction with 5 steps

1.1: 84 percent / Br₂ / CHCl₃

2.1: 97 percent / K₂CO₃ / dimethylformamide

3.1: s-BuLi / tetrahydrofuran

3.2: 41 percent / tetrahydrofuran

4.1: 100 percent / IBX / toluene; dimethylsulfoxide

5.1: 88 percent / HCO₂NH₄; Pd/C / acetone

With palladium on activated charcoal; bromine; sec.-butyllithium; ammonium formate; potassium carbonate; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; chloroform; dimethyl sulfoxide; N,N-dimethyl-formamide; acetone; toluene;
DOI:10.1016/S0960-894X(03)00719-4

Reference yield:

: 13246-46-3
2,4-dibenzyloxybenzaldehyde

: 622390-73-2
[4,6-dihydroxy-2-methoxymethoxy-3-(3-methyl-but-2-enyl)-phenyl]-(2,4-dihydroxy-5-methoxy-phenyl)-methanone

Guidance literature:: Multi-step reaction with 7 steps

1.1: mCPBA / CH₂Cl₂

2.1: aq. HCl / methanol

3.1: 84 percent / Br₂ / CHCl₃

4.1: 97 percent / K₂CO₃ / dimethylformamide

5.1: s-BuLi / tetrahydrofuran

5.2: 41 percent / tetrahydrofuran

6.1: 100 percent / IBX / toluene; dimethylsulfoxide

7.1: 88 percent / HCO₂NH₄; Pd/C / acetone

With hydrogenchloride; palladium on activated charcoal; bromine; sec.-butyllithium; ammonium formate; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; methanol; dichloromethane; chloroform; dimethyl sulfoxide; N,N-dimethyl-formamide; acetone; toluene; 1.1: Baeyer-Villiger oxidation;
DOI:10.1016/S0960-894X(03)00719-4