N-4-nitrophenyl sulfonamido homopropargyl amine

Base Information

Chemical Name:N-4-nitrophenyl sulfonamido homopropargyl amine
CAS No.:1035148-61-8
Molecular Formula:C₁₀H₁₀N₂O₄S
Molecular Weight:254.266
Hs Code.:

Synonyms:N-4-nitrophenyl sulfonamido homopropargyl amine

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Chemical Property of N-4-nitrophenyl sulfonamido homopropargyl amine

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Technology Process of N-4-nitrophenyl sulfonamido homopropargyl amine

There total 3 articles about N-4-nitrophenyl sulfonamido homopropargyl amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 14044-63-4
but-3-yn-1-amine

: 98-74-8
4-Nitrobenzenesulfonyl chloride

: 1035148-61-8
N-4-nitrophenyl sulfonamido homopropargyl amine

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1002/ejoc.200901372

Reference yield:

: C₁₅H₁₈N₂O₆S

: 1035148-61-8
N-4-nitrophenyl sulfonamido homopropargyl amine

Guidance literature:: With trifluoroacetic acid; In dichloromethane; for 4h; Inert atmosphere;
DOI:10.1021/jo802582k

Reference yield:

: 895153-23-8
N-(tert-butoxycarbonyl)-4-nitrobenzenesulfonamide

: 1035148-61-8
N-4-nitrophenyl sulfonamido homopropargyl amine

Guidance literature:: Multi-step reaction with 2 steps

1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0 - 20 °C

2: trifluoroacetic acid / dichloromethane / 0 - 20 °C

With di-isopropyl azodicarboxylate; triphenylphosphine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1039/d1cc04830a