pentacarbonyl-(μ-di-tert-butylphosphido)-(μ-dicyclohexylphosphido)diiron

Base Information

Chemical Name:pentacarbonyl-(μ-di-tert-butylphosphido)-(μ-dicyclohexylphosphido)diiron
CAS No.:140657-01-8
Molecular Formula:C₂₅H₄₀Fe₂O₅P₂
Molecular Weight:594.231
Hs Code.:

Synonyms:pentacarbonyl-(μ-di-tert-butylphosphido)-(μ-dicyclohexylphosphido)diiron

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Chemical Property of pentacarbonyl-(μ-di-tert-butylphosphido)-(μ-dicyclohexylphosphido)diiron

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Technology Process of pentacarbonyl-(μ-di-tert-butylphosphido)-(μ-dicyclohexylphosphido)diiron

There total 2 articles about pentacarbonyl-(μ-di-tert-butylphosphido)-(μ-dicyclohexylphosphido)diiron which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 140633-99-4
hexacarbonyl-(μ-di-tert-butylphosphido)-(μ-dicyclohexylphosphido)diiron

: 140657-01-8
pentacarbonyl-(μ-di-tert-butylphosphido)-(μ-dicyclohexylphosphido)diiron

Guidance literature:: In n-heptane; byproducts: CO; Irradiation (UV/VIS); a photoreactor is charged with Fe-complex in heptane, photolyzation for 90 min under Ar; isolation of product is described in: Walther, B., Hartung, H., Reinhold, J.; Jones, P. G., Boettcher, H.C., Baumeister, U., Krug, A. Chem. Ber. 1992, 125 1379;

Reference yield:

: 16523-54-9
chlorodicyclohexylphosphane

: 140657-01-8
pentacarbonyl-(μ-di-tert-butylphosphido)-(μ-dicyclohexylphosphido)diiron

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran

2: toluene

In tetrahydrofuran; toluene;

Reference yield: 100.0%

: 140657-01-8
pentacarbonyl-(μ-di-tert-butylphosphido)-(μ-dicyclohexylphosphido)diiron

: 2071-20-7
bis-diphenylphosphinomethane

: [Fe₂(CO)5(P(C(CH₃)3)2)(P((CH(CH₂)5))2)((C₆H₅)2PCH₂P(C₆H₅)2)]*0.5C₄H₈O

Guidance literature:: In tetrahydrofuran; (Ar); stirring (25°C, 2 h); solvent removal (vac.), extracting (pentane), filtn., solvent redn. (vac.), crystn. (-30°C); elem. anal.;
DOI:10.1016/0277-5387(94)00319-A