2-<(2-chloro-3-pyridinyl)carbonyl>-1-cyclohexen-1-yl-2-chloro-3-pyridinecarboxylate

Base Information

• Chemical Name: 2-<(2-chloro-3-pyridinyl)carbonyl>-1-cyclohexen-1-yl-2-chloro-3-pyridinecarboxylate
• CAS No.: 153615-34-0
• Molecular Formula: C₁₈H₁₄Cl₂N₂O₃
• Molecular Weight: 377.227

Synonyms:2-<(2-chloro-3-pyridinyl)carbonyl>-1-cyclohexen-1-yl-2-chloro-3-pyridinecarboxylate

Chemical Property of 2-<(2-chloro-3-pyridinyl)carbonyl>-1-cyclohexen-1-yl-2-chloro-3-pyridinecarboxylate

Chemical Property:

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Technology Process of 2-<(2-chloro-3-pyridinyl)carbonyl>-1-cyclohexen-1-yl-2-chloro-3-pyridinecarboxylate

There total 4 articles about 2-<(2-chloro-3-pyridinyl)carbonyl>-1-cyclohexen-1-yl-2-chloro-3-pyridinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

4-cyclohexen-1-ylmorpholine (670-80-4) + 2-Chloronicotinoyl chloride (49609-84-9) → 2-<(2-chloro-3-pyridinyl)carbonyl>-1-cyclohexen-1-yl-2-chloro-3-pyridinecarboxylate (153615-34-0)

Guidance literature:

With triethylamine; In dichloromethane; at 25 ℃; for 118h;

DOI:10.1016/S0040-4020(01)87197-0

Reference yield:

(2-chloro-3-pyridinyl)<2-(4-morpholinyl)-1-cyclohexen-1-yl>methanone (110545-74-9) → 2-<(2-chloro-3-pyridinyl)carbonyl>-1-cyclohexen-1-yl-2-chloro-3-pyridinecarboxylate (153615-34-0)

Guidance literature:

With silica gel; In dichloromethane; Yield given;

DOI:10.1016/S0040-4020(01)87197-0

Reference yield:

4-cyclohexen-1-ylmorpholine (670-80-4) → 2-<(2-chloro-3-pyridinyl)carbonyl>-1-cyclohexen-1-yl-2-chloro-3-pyridinecarboxylate (153615-34-0)

Guidance literature:

Multi-step reaction with 2 steps

1: NEt₃ / CH₂Cl₂ / 1.) 1.25 h; 2.) 1 h

2: silica gel / CH₂Cl₂

With silica gel; triethylamine; In dichloromethane;

DOI:10.1016/S0040-4020(01)87197-0

upstream raw materials:

4-cyclohexen-1-ylmorpholine

2-Chloronicotinoyl chloride

(2-chloro-3-pyridinyl)<2-(4-morpholinyl)-1-cyclohexen-1-yl>methanone

Downstream raw materials:

10-(3-Chlorophenyl)-6,8,9,10-tetrahydrobenzo<1,8>naphthyridin-5(7H)-one

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