[Li₂(o-C₆H₄PPh₂NPh)₂]OEt₂

Base Information

Chemical Name:[Li₂(o-C₆H₄PPh₂NPh)₂]OEt₂
CAS No.:663627-50-7
Molecular Formula:C₅₂H₄₈Li₂N₂OP₂
Molecular Weight:792.795
Hs Code.:

[Li<sub>2</sub>(o-C<sub>6</sub>H<sub>4</sub>PPh<sub>2</sub>NPh)<sub>2</sub>]OEt<sub>2</sub>

Synonyms:[Li₂(o-C₆H₄PPh₂NPh)₂]OEt₂

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Chemical Property of [Li₂(o-C₆H₄PPh₂NPh)₂]OEt₂

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Technology Process of [Li₂(o-C₆H₄PPh₂NPh)₂]OEt₂

There total 1 articles about [Li₂(o-C₆H₄PPh₂NPh)₂]OEt₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 60-29-7,927820-24-4
diethyl ether

: 591-51-5
phenyllithium

: 2325-27-1
N-phenyltriphenyliminophosphorane

: 663627-50-7
[Li₂(o-C₆H₄PPh₂NPh)₂]OEt₂

Guidance literature:: Inert atmosphere; Schlenk technique;
DOI:10.1016/j.jorganchem.2014.05.024

Reference yield: 74.0%

: 36673-36-6,111408-20-9,14126-37-5,54053-52-0
dibromobis(triphenylphosphine)nickel(II)

: 663627-50-7
[(o-C₆H₄PPh₂NPh)Li]2*Et₂O

: 690634-62-9
[Ni(o-C₆H₄PPh₂NPh)2]

Guidance literature:: In tetrahydrofuran; (N2); a soln. of Li compd. and Ni complex dissolved in THF at -20°C, stirred overnight at 25°C; evapn. (vac.), washing with pentane, recrystn. (benzene); elem. anal.;
DOI:10.1039/b305877h

Reference yield: 67.0%

: 12112-67-3
bis(1,5-cyclooctadiene)diiridium(I) dichloride

: 663627-50-7
[Li₂(o-C₆H₄PPh₂NPh)₂]OEt₂

: 663627-59-6
Ir(cyclooctadiene)(o-C₆H₄P(phenyl)2N(phenyl))

Guidance literature:: In tetrahydrofuran; N2; dissolving Ir complex and the organolithium compd. in THF at 25°C, stirring overnight; solvent removal in vac., washing the residue with pentane, recrystn. from THD/diethyl ether or THF/C6H6; elem. anal.;
DOI:10.1021/om030539g