phenylcarbamoylacetamidooxime O-mesylate

Base Information

Chemical Name:phenylcarbamoylacetamidooxime O-mesylate
CAS No.:102926-35-2
Molecular Formula:C₁₀H₁₃N₃O₄S
Molecular Weight:271.297
Hs Code.:

Synonyms:phenylcarbamoylacetamidooxime O-mesylate

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Chemical Property of phenylcarbamoylacetamidooxime O-mesylate

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Technology Process of phenylcarbamoylacetamidooxime O-mesylate

There total 3 articles about phenylcarbamoylacetamidooxime O-mesylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 61239-31-4
3-amino-3-(hydroxyimino)-N-phenylpropanamide

: 124-63-0
methanesulfonyl chloride

: 102926-35-2
phenylcarbamoylacetamidooxime O-mesylate

Guidance literature:: In pyridine; 1) -20 deg C, 15 min 2) 0 deg C, 20 min;
DOI:10.1007/BF00515022

Reference yield:

: 621-03-4
cyanoacetanilide

: 102926-35-2
phenylcarbamoylacetamidooxime O-mesylate

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / NH₂OH*HCl, sodium carbonate / aq. ethanol / 1) 70 deg C, 45 min 2) RT, overnight

2: 72 percent / pyridine / 1) -20 deg C, 15 min 2) 0 deg C, 20 min

With hydroxylamine hydrochloride; sodium carbonate; In pyridine; ethanol;
DOI:10.1007/BF00515022

Reference yield:

: 62-53-3
aniline

: 102926-35-2
phenylcarbamoylacetamidooxime O-mesylate

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / neat (no solvent) / 180 - 190 °C

2: 62 percent / NH₂OH*HCl, sodium carbonate / aq. ethanol / 1) 70 deg C, 45 min 2) RT, overnight

3: 72 percent / pyridine / 1) -20 deg C, 15 min 2) 0 deg C, 20 min

With hydroxylamine hydrochloride; sodium carbonate; In pyridine; ethanol;
DOI:10.1007/BF00515022