1-[(1S,2S)-1,2-Bis-benzyloxy-2-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-ethyl]-cyclopropanecarbaldehyde

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Chemical Name:1-[(1S,2S)-1,2-Bis-benzyloxy-2-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-ethyl]-cyclopropanecarbaldehyde
CAS No.:133463-16-8
Molecular Formula:C₂₅H₃₀O₅
Molecular Weight:410.51
Hs Code.:

Synonyms:1-[(1S,2S)-1,2-Bis-benzyloxy-2-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-ethyl]-cyclopropanecarbaldehyde

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Chemical Property of 1-[(1S,2S)-1,2-Bis-benzyloxy-2-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-ethyl]-cyclopropanecarbaldehyde

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Technology Process of 1-[(1S,2S)-1,2-Bis-benzyloxy-2-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-ethyl]-cyclopropanecarbaldehyde

There total 8 articles about 1-[(1S,2S)-1,2-Bis-benzyloxy-2-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-ethyl]-cyclopropanecarbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 133463-13-5
{1-[(1S,2S)-1,2-Bis-benzyloxy-2-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-ethyl]-cyclopropyl}-methanol

: 133463-16-8
1-[(1S,2S)-1,2-Bis-benzyloxy-2-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-ethyl]-cyclopropanecarbaldehyde

Guidance literature:: With pyridinium chlorochromate; In dichloromethane;
DOI:10.1016/S0040-4039(00)79465-2

Reference yield: 48.0%

: 133522-01-7
{1-[(1R,2S)-1,2-Bis-benzyloxy-2-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-ethyl]-cyclopropyl}-methanol

: 133463-16-8
1-[(1R,2S)-1,2-Bis-benzyloxy-2-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-ethyl]-cyclopropanecarbaldehyde

Guidance literature:: With pyridinium chlorochromate; In dichloromethane;
DOI:10.1016/S0040-4039(00)79465-2

Reference yield:

: 1-[(S)-1,2-Bis-benzyloxy-2-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-ethyl]-cyclopropanecarboxylic acid 2,6-di-tert-butyl-4-methyl-phenyl ester

: 133463-16-8
1-[(1S,2S)-1,2-Bis-benzyloxy-2-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-ethyl]-cyclopropanecarbaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: LiAlH₄ / tetrahydrofuran / 168 h / Heating

2: 74 percent / pyridinium chlorochromate (PCC) / CH₂Cl₂

With lithium aluminium tetrahydride; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4039(00)79465-2